6-Azido-1,3-dimethyl-5-phenylpyrimidine-2,4(1H,3H)-dione

Base Information

• Chemical Name: 6-Azido-1,3-dimethyl-5-phenylpyrimidine-2,4(1H,3H)-dione
• CAS No.: 89549-99-5
• Molecular Formula: C12H11N5O2
• Molecular Weight: 257.252
• DSSTox Substance ID: DTXSID50529690
• Wikidata: Q82400297

Synonyms:89549-99-5;DTXSID50529690;6-Azido-1,3-dimethyl-5-phenylpyrimidine-2,4(1H,3H)-dione

Chemical Property of 6-Azido-1,3-dimethyl-5-phenylpyrimidine-2,4(1H,3H)-dione

Chemical Property:

• XLogP3: 2.2
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 2
• Exact Mass: 257.09127461
• Heavy Atom Count: 19
• Complexity: 486

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CN1C(=C(C(=O)N(C1=O)C)C2=CC=CC=C2)N=[N+]=[N-]

Technology Process of 6-Azido-1,3-dimethyl-5-phenylpyrimidine-2,4(1H,3H)-dione

There total 1 articles about 6-Azido-1,3-dimethyl-5-phenylpyrimidine-2,4(1H,3H)-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

6-chloro-1,3-dimethyl-5-phenyl-pyrimidine-2,4(1H,3H)-dione (51759-18-3) → 6-azido-1,3-dimethyl-5-phenyl-pyrimidine-2,4(1H,3H)-dione (89549-99-5)

Guidance literature:

With sodium azide; In N,N-dimethyl-formamide; for 12h; Ambient temperature;

DOI:10.1007/BF00810091

Reference yield: 90.0%

6-azido-1,3-dimethyl-5-phenyl-pyrimidine-2,4(1H,3H)-dione (89549-99-5) + triphenylphosphine (603-35-0) → 1,3-dimethyl-6-triphenylphosphoranylideneamino-5-phenyl-pyrimidine-2,4(1H,3H)-dione (115127-17-8)

Guidance literature:

In benzene; for 2h; Heating;

DOI:10.1007/BF00810091

Reference yield: 77.0%

6-azido-1,3-dimethyl-5-phenyl-pyrimidine-2,4(1H,3H)-dione (89549-99-5) → 6-amino-1,3-dimethyl-5-phenyl-pyridino-2,4(1H,3H)-dione (100193-79-1)

Guidance literature:

With hydrogen; palladium on activated charcoal; In methanol; for 4h; Ambient temperature;

DOI:10.1007/BF00810091

upstream raw materials:

6-chloro-1,3-dimethyl-5-phenyl-pyrimidine-2,4(1H,3H)-dione

Downstream raw materials:

6-amino-1,3-dimethyl-5-phenyl-pyridino-2,4(1H,3H)-dione

1,3-dimethyl-6-triphenylphosphoranylideneamino-5-phenyl-pyrimidine-2,4(1H,3H)-dione

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