1,3-Dimethyl-5-phenyl-6-[(triphenylphosphoranylidene)amino]-2,4(1H,3H)-pyrimidinedione

Base Information

Chemical Name:1,3-Dimethyl-5-phenyl-6-[(triphenylphosphoranylidene)amino]-2,4(1H,3H)-pyrimidinedione
CAS No.:115127-17-8
Molecular Formula:C₃₀H₂₆N₃O₂P
Molecular Weight:491.529
Hs Code.:
DSSTox Substance ID:DTXSID301125890

Synonyms:DTXSID301125890;1,3-Dimethyl-5-phenyl-6-[(triphenylphosphoranylidene)amino]-2,4(1H,3H)-pyrimidinedione;115127-17-8

Suppliers and Price of 1,3-Dimethyl-5-phenyl-6-[(triphenylphosphoranylidene)amino]-2,4(1H,3H)-pyrimidinedione

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,3-Dimethyl-5-phenyl-6-[(triphenylphosphoranylidene)amino]-2,4(1H,3H)-pyrimidinedione

Chemical Property:

XLogP3:5.8
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:5
Exact Mass:491.17626408
Heavy Atom Count:36
Complexity:836

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CN1C(=C(C(=O)N(C1=O)C)C2=CC=CC=C2)N=P(C3=CC=CC=C3)(C4=CC=CC=C4)C5=CC=CC=C5

Technology Process of 1,3-Dimethyl-5-phenyl-6-[(triphenylphosphoranylidene)amino]-2,4(1H,3H)-pyrimidinedione

There total 2 articles about 1,3-Dimethyl-5-phenyl-6-[(triphenylphosphoranylidene)amino]-2,4(1H,3H)-pyrimidinedione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 89549-99-5
6-azido-1,3-dimethyl-5-phenyl-pyrimidine-2,4(1H,3H)-dione

: 603-35-0
triphenylphosphine

: 115127-17-8
1,3-dimethyl-6-triphenylphosphoranylideneamino-5-phenyl-pyrimidine-2,4(1H,3H)-dione

Guidance literature:: In benzene; for 2h; Heating;
DOI:10.1007/BF00810091

Reference yield:

: 51759-18-3
6-chloro-1,3-dimethyl-5-phenyl-pyrimidine-2,4(1H,3H)-dione

: 115127-17-8
1,3-dimethyl-6-triphenylphosphoranylideneamino-5-phenyl-pyrimidine-2,4(1H,3H)-dione

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / NaN₃ / dimethylformamide / 12 h / Ambient temperature

2: 90 percent / benzene / 2 h / Heating

With sodium azide; In N,N-dimethyl-formamide; benzene;
DOI:10.1007/BF00810091