4-(3,4-Dichlorobenzamido)benzene-1-sulfonyl chloride

Base Information

Chemical Name:4-(3,4-Dichlorobenzamido)benzene-1-sulfonyl chloride
CAS No.:89564-67-0
Molecular Formula:C13H8Cl3NO3S
Molecular Weight:364.636
Hs Code.:
DSSTox Substance ID:DTXSID20536513
Wikidata:Q82411208

Synonyms:89564-67-0;4-(3,4-Dichlorobenzamido)benzene-1-sulfonyl chloride;DTXSID20536513;AKOS009147235

Suppliers and Price of 4-(3,4-Dichlorobenzamido)benzene-1-sulfonyl chloride

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-(3,4-Dichlorobenzamido)benzene-1-sulfonyl chloride

Chemical Property:

XLogP3:4.4
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:3
Exact Mass:362.929047
Heavy Atom Count:21
Complexity:472

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC(=CC=C1NC(=O)C2=CC(=C(C=C2)Cl)Cl)S(=O)(=O)Cl

Technology Process of 4-(3,4-Dichlorobenzamido)benzene-1-sulfonyl chloride

There total 3 articles about 4-(3,4-Dichlorobenzamido)benzene-1-sulfonyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 6043-42-1
3,4-dichloro-N-phenylbenzamide

: 89564-67-0
4-(3,4-Dichloro-benzoylamino)-benzenesulfonyl chloride

Guidance literature:: With chlorosulfonic acid; at 40 - 60 ℃; for 3h;

Reference yield:

: potassium 4-(3,4-dichlorobenzamido)benzenesulfonate

: 89564-67-0
4-(3,4-Dichloro-benzoylamino)-benzenesulfonyl chloride

Guidance literature:: With oxalyl dichloride; In dichloromethane; N,N-dimethyl-formamide; at 0 - 40 ℃; for 3h;
DOI:10.1016/j.ejmech.2019.111789

Reference yield:

: 121-57-3,856062-06-1
4-aminobenzene sulfonic acid

: 89564-67-0
4-(3,4-Dichloro-benzoylamino)-benzenesulfonyl chloride

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / water; tetrahydrofuran / 20 °C

2: oxalyl dichloride / N,N-dimethyl-formamide; dichloromethane / 3 h / 0 - 40 °C

With oxalyl dichloride; potassium carbonate; In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1016/j.ejmech.2019.111789