1-Hydroxy-5,6,6-trimethyl-4-oxo-3,6-dihydro-4lambda~5~-pyrazin-2(1H)-one

Base Information

Chemical Name:1-Hydroxy-5,6,6-trimethyl-4-oxo-3,6-dihydro-4lambda~5~-pyrazin-2(1H)-one
CAS No.:89587-36-0
Molecular Formula:C₇H₁₂N₂O₃
Molecular Weight:172.184
Hs Code.:
DSSTox Substance ID:DTXSID40528733
Wikidata:Q82398582

Synonyms:89587-36-0;DTXSID40528733;1-Hydroxy-5,6,6-trimethyl-4-oxo-3,6-dihydro-4lambda~5~-pyrazin-2(1H)-one

Suppliers and Price of 1-Hydroxy-5,6,6-trimethyl-4-oxo-3,6-dihydro-4lambda~5~-pyrazin-2(1H)-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-Hydroxy-5,6,6-trimethyl-4-oxo-3,6-dihydro-4lambda~5~-pyrazin-2(1H)-one

Chemical Property:

Boiling Point:339.1±52.0 °C(Predicted)
PSA：69.29000
Density:1.26±0.1 g/cm3(Predicted)
LogP:-0.13570
XLogP3:-1.7
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:0
Exact Mass:172.08479225
Heavy Atom Count:12
Complexity:257

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC1=[N+](CC(=O)N(C1(C)C)O)[O-]

Technology Process of 1-Hydroxy-5,6,6-trimethyl-4-oxo-3,6-dihydro-4lambda~5~-pyrazin-2(1H)-one

There total 2 articles about 1-Hydroxy-5,6,6-trimethyl-4-oxo-3,6-dihydro-4lambda~5~-pyrazin-2(1H)-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 89587-27-9
N-(1,1-Dimethyl-2-hydroxyiminopropyl)-2-chloroacethydroxamic acid

: 89587-36-0
1-Hydroxy-5,6,6-trimethyl-4-oxy-3,6-dihydro-1H-pyrazin-2-one

Guidance literature:: With sodium ethanolate; In ethanol; for 1h;
DOI:10.1007/BF00505860

Reference yield:

: 38870-64-3
3-hydroxyamino-3-methyl-butan-2-one oxime

: 89587-36-0
1-Hydroxy-5,6,6-trimethyl-4-oxy-3,6-dihydro-1H-pyrazin-2-one

Guidance literature:: Multi-step reaction with 2 steps

1: 44 percent / Triethylamine / tetrahydrofuran / 2.58 h / Ice bath

2: 83 percent / Sodium ethanolate / ethanol / 1 h

With sodium ethanolate; triethylamine; In tetrahydrofuran; ethanol;
DOI:10.1007/BF00505860