2-(Chloromethyl)-4-methyl-1,3-dioxane

Base Information

Chemical Name:2-(Chloromethyl)-4-methyl-1,3-dioxane
CAS No.:6414-14-8
Molecular Formula:C₆H₁₁ClO₂
Molecular Weight:150.605
Hs Code.:
NSC Number:75245
DSSTox Substance ID:DTXSID30291404

Synonyms:6414-14-8;2-(chloromethyl)-4-methyl-1,3-dioxane;NSC75245;SCHEMBL10973909;DTXSID30291404;NSC-75245;AKOS006387367

Suppliers and Price of 2-(Chloromethyl)-4-methyl-1,3-dioxane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of 2-(Chloromethyl)-4-methyl-1,3-dioxane

Chemical Property:

Vapor Pressure:0.661mmHg at 25°C
Boiling Point:193°Cat760mmHg
Flash Point:70.4°C
Density:1.068g/cm³
XLogP3:1.2
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:1
Exact Mass:150.0447573
Heavy Atom Count:9
Complexity:87.1

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1CCOC(O1)CCl

Technology Process of 2-(Chloromethyl)-4-methyl-1,3-dioxane

There total 2 articles about 2-(Chloromethyl)-4-methyl-1,3-dioxane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 18826-95-4,107-88-0
1.3-butanediol

: 97-97-2
chloroacetaldehyde dimethyl acetal

: 6414-14-8
2-chloromethyl-4-methyl-1,3-dioxane

Guidance literature:: DOI:10.1021/jo990227g

Reference yield:

: 6414-14-8
2-chloromethyl-4-methyl-1,3-dioxane

Guidance literature:: 2,4-Butandiol, Chloracetaldehyddimethylacetal, konz. H2SO4;

Reference yield:

: 6414-14-8
2-chloromethyl-4-methyl-1,3-dioxane

: 1-methyl-3-acetoxypropyl benzoate

Guidance literature:: Multi-step reaction with 2 steps

1: 75 percent / potassium tert-butoxide; Aliquat 336 / tetrahydrofuran / 20 °C / Heating

2: tetrahydrofuran / 4 h / 20 °C

With potassium tert-butylate; Aliquat 336; In tetrahydrofuran; 1: Dehydrochlorination / 2: Acylation;
DOI:10.1021/jo990227g