Benzene, 2,3-dimethoxy-1,4-bis(phenylmethoxy)-

Base Information

Chemical Name:Benzene, 2,3-dimethoxy-1,4-bis(phenylmethoxy)-
CAS No.:89635-20-1
Molecular Formula:C22H22O4
Molecular Weight:350.414
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Benzene, 2,3-dimethoxy-1,4-bis(phenylmethoxy)-

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

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Technology Process of Benzene, 2,3-dimethoxy-1,4-bis(phenylmethoxy)-

There total 4 articles about Benzene, 2,3-dimethoxy-1,4-bis(phenylmethoxy)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 36.0%

: 52643-52-4
2,3-dimethoxybenzene-1,4-diol

: 100-39-0
benzyl bromide

: 89635-20-1
1,4-bis(benzyloxy)-2,3-dimethoxybenzene

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide;

Reference yield:

: 2103-57-3
2,3,4-trimethoxybenzaldehyde

: 89635-20-1
1,4-bis(benzyloxy)-2,3-dimethoxybenzene

Guidance literature:: Multi-step reaction with 5 steps

1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 3 h / 0 - 20 °C

2: sodium hydroxide / methanol; water / 16 h / 20 °C

3: ammonium cerium (IV) nitrate; silica gel / dichloromethane; water / 20 °C

4: sodium tetrahydroborate / methanol; water; diethyl ether / 2 h / 20 °C

5: caesium carbonate / N,N-dimethyl-formamide / 16 h / 90 °C

With sodium tetrahydroborate; ammonium cerium (IV) nitrate; silica gel; caesium carbonate; 3-chloro-benzenecarboperoxoic acid; sodium hydroxide; In methanol; diethyl ether; dichloromethane; water; N,N-dimethyl-formamide; 1: |Baeyer-Villiger Ketone Oxidation;
DOI:10.1021/acs.orglett.8b00340

Reference yield:

: 3117-02-0
2,3-dimethoxy-1,4-benzoquinone

: 89635-20-1
1,4-bis(benzyloxy)-2,3-dimethoxybenzene

Guidance literature:: Multi-step reaction with 2 steps

1: sodium tetrahydroborate / methanol; water; diethyl ether / 2 h / 20 °C

2: caesium carbonate / N,N-dimethyl-formamide / 16 h / 90 °C

With sodium tetrahydroborate; caesium carbonate; In methanol; diethyl ether; water; N,N-dimethyl-formamide;
DOI:10.1021/acs.orglett.8b00340