1'-Isoemetine

Base Information

Chemical Name:1'-Isoemetine
CAS No.:522-99-6
Molecular Formula:C29H40N2O4
Molecular Weight:480.648
Hs Code.:
Mol file:522-99-6.mol

Synonyms:

Suppliers and Price of 1'-Isoemetine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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Total 0 raw suppliers

Chemical Property of 1'-Isoemetine

Chemical Property:

Boiling Point:600.3°Cat760mmHg
Flash Point:316.9°C
Density:1.17g/cm³

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 1'-Isoemetine

There total 43 articles about 1'-Isoemetine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 163926-93-0
N-Pent-4-enoylemetine

: 483-18-1,522-99-6,7005-82-5,38241-16-6,65910-27-2,74059-23-7,74111-75-4,74111-76-5
emetine

Guidance literature:: With iodine; In tetrahydrofuran; water;
DOI:10.1021/ja00116a047

Reference yield: 72.0%

: 523-01-3
(-)-2-(6,7-dimethoxy-3,4-dihydroisoquinolin-1-ylmethyl)-3-ethyl-9,10-dimethoxy-1,3,4,6,7,11b-hexahydro-2H-pyrido[2,1-a]isoquinoline

: 483-18-1,522-99-6,7005-82-5,38241-16-6,65910-27-2,74059-23-7,74111-75-4,74111-76-5
emetine

Guidance literature:: With formic acid; triethylamine; Cl[(1S,2S)-N-p-Ts-1,2-diphenylethanediamine](p-cymene)Ru(II); In N,N-dimethyl-formamide; at 20 ℃; for 3.3h;
DOI:10.1021/ol0530326

Reference yield:

: 120-20-7
2-(3,4-dimethoxyphenyl)-ethylamine

: 483-18-1,522-99-6,7005-82-5,38241-16-6,65910-27-2,74059-23-7,74111-75-4,74111-76-5
emetine

Guidance literature:: Multi-step reaction with 3 steps

1: 73 percent / AlMe₃ / benzene / 10 h / 115 °C

2: 75 percent / POCl₃ / benzene / 3.8 h / 110 °C

3: 72 percent / HCO₂H; Et₃N / Cl[(1S,2S)-N-p-Ts-1,2-diphenylethanediamine](p-cymene)Ru(II) / dimethylformamide / 3.3 h / 20 °C

With formic acid; trimethylaluminum; triethylamine; trichlorophosphate; Cl[(1S,2S)-N-p-Ts-1,2-diphenylethanediamine](p-cymene)Ru(II); In N,N-dimethyl-formamide; benzene;
DOI:10.1021/ol0530326