2-[(3-Bromo-4-methoxyphenyl)methyl]-1,4-dimethylbenzene

Base Information

Chemical Name:2-[(3-Bromo-4-methoxyphenyl)methyl]-1,4-dimethylbenzene
CAS No.:89651-85-4
Molecular Formula:C16H17BrO
Molecular Weight:305.214
Hs Code.:
DSSTox Substance ID:DTXSID40529508
Wikidata:Q82399963

Synonyms:89651-85-4;2-[(3-Bromo-4-methoxyphenyl)methyl]-1,4-dimethylbenzene;DTXSID40529508

Suppliers and Price of 2-[(3-Bromo-4-methoxyphenyl)methyl]-1,4-dimethylbenzene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-[(3-Bromo-4-methoxyphenyl)methyl]-1,4-dimethylbenzene

Chemical Property:

XLogP3:5.2
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:3
Exact Mass:304.04628
Heavy Atom Count:18
Complexity:256

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC1=CC(=C(C=C1)C)CC2=CC(=C(C=C2)OC)Br

Technology Process of 2-[(3-Bromo-4-methoxyphenyl)methyl]-1,4-dimethylbenzene

There total 5 articles about 2-[(3-Bromo-4-methoxyphenyl)methyl]-1,4-dimethylbenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 89651-84-3
3-bromo-4-hydroxy-2',5'-dimethylphenylmethane

: 74-88-4
methyl iodide

: 89651-85-4
3-bromo-4-methoxy-2',5'-dimethyldiphenylmethane

Guidance literature:: With potassium carbonate; In acetone; for 2.5h; Heating;
DOI:10.1016/S0040-4020(01)88629-4

Reference yield:

: 578-57-4
2-bromoanisole

: 89651-85-4
3-bromo-4-methoxy-2',5'-dimethyldiphenylmethane

Guidance literature:: Multi-step reaction with 3 steps

1: 58.5 percent / imidazole, trifluoroacetic anhydride / trifluoroacetic acid / 18 h / Heating

2: 65 percent / KOH, hydrazine hydrate / bis-(2-hydroxy-ethyl) ether / 2 h / Heating

3: 85 percent / K₂CO₃ / acetone / 2.5 h / Heating

With 1H-imidazole; potassium hydroxide; potassium carbonate; hydrazine hydrate; trifluoroacetic anhydride; In acetone; trifluoroacetic acid; diethylene glycol;
DOI:10.1016/S0040-4020(01)88629-4

Reference yield:

: 89651-83-2
3-bromo-4-methoxy-2',5'-dimethylbenzophenone

: 89651-85-4
3-bromo-4-methoxy-2',5'-dimethyldiphenylmethane

Guidance literature:: Multi-step reaction with 2 steps

1: 65 percent / KOH, hydrazine hydrate / bis-(2-hydroxy-ethyl) ether / 2 h / Heating

2: 85 percent / K₂CO₃ / acetone / 2.5 h / Heating

With potassium hydroxide; potassium carbonate; hydrazine hydrate; In acetone; diethylene glycol;
DOI:10.1016/S0040-4020(01)88629-4