(E)-1-(2-Benzylpiperidin-1-yl)-N-tert-butylmethanimine

Base Information

Chemical Name:(E)-1-(2-Benzylpiperidin-1-yl)-N-tert-butylmethanimine
CAS No.:89656-42-8
Molecular Formula:C17H26N2
Molecular Weight:258.407
Hs Code.:
DSSTox Substance ID:DTXSID60534634

Synonyms:89656-42-8;(E)-1-(2-Benzylpiperidin-1-yl)-N-tert-butylmethanimine;DTXSID60534634

Suppliers and Price of (E)-1-(2-Benzylpiperidin-1-yl)-N-tert-butylmethanimine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemical Property of (E)-1-(2-Benzylpiperidin-1-yl)-N-tert-butylmethanimine

Chemical Property:

PSA：15.60000
LogP:3.84830
XLogP3:3.7
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:4
Exact Mass:258.209598838
Heavy Atom Count:19
Complexity:284

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(C)(C)N=CN1CCCCC1CC2=CC=CC=C2

Technology Process of (E)-1-(2-Benzylpiperidin-1-yl)-N-tert-butylmethanimine

There total 3 articles about (E)-1-(2-Benzylpiperidin-1-yl)-N-tert-butylmethanimine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 119044-70-1
(E)-N′-tert-butyl-N,N-dimethylformimidamide

: 89656-42-8
[1-(2-Benzyl-piperidin-1-yl)-meth-(E)-ylidene]-tert-butyl-amine

Guidance literature:: Multi-step reaction with 2 steps

1: 93 percent / (NH₄)2SO₄ / toluene / Heating

2: 1.) t-BuLi; 2.) pentynylcopper / 1.) THF, -20 deg C, 1 h; 2.) THF, -20 deg C

With 1-pentynyl copper; ammonium sulfate; tert.-butyl lithium; In toluene;
DOI:10.1021/ja00323a035

Reference yield:

: 100-39-0
benzyl bromide

: 85152-52-9
N-(N'-tert-butylformimidoyl)piperidine

: 89656-42-8
[1-(2-Benzyl-piperidin-1-yl)-meth-(E)-ylidene]-tert-butyl-amine

Guidance literature:: With 1-pentynyl copper; tert.-butyl lithium; Yield given. Multistep reaction; 1.) THF, -20 deg C, 1 h; 2.) THF, -20 deg C;
DOI:10.1021/ja00323a035

Reference yield:

: 131248-73-2
2-methoxy piperidine N-t-butyl formamidine

: 6921-34-2
benzylmagnesium chloride

: 89656-42-8
[1-(2-Benzyl-piperidin-1-yl)-meth-(E)-ylidene]-tert-butyl-amine

Guidance literature:: In diethyl ether; for 12h; Ambient temperature; also with 2-methoxy pyrrolidine N-t-butyl formamide, various grignard reagents;
DOI:10.1016/S0040-4039(00)97716-5