1-tert-Butyl-4-(cyclohexylmethylidene)cyclohexane

Base Information

Chemical Name:1-tert-Butyl-4-(cyclohexylmethylidene)cyclohexane
CAS No.:89657-03-4
Molecular Formula:C17H30
Molecular Weight:234.425
Hs Code.:
DSSTox Substance ID:DTXSID60534336

Synonyms:89657-03-4;1-tert-Butyl-4-(cyclohexylmethylidene)cyclohexane;DTXSID60534336;AKOS015907436;1-tert-butyl-4-(cyclohexylmethylene)cyclohexane;1-tert-butyl-4-(cyclohexyl-methylene)-cyclohexane

Suppliers and Price of 1-tert-Butyl-4-(cyclohexylmethylidene)cyclohexane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-tert-Butyl-4-(cyclohexylmethylidene)cyclohexane

Chemical Property:

XLogP3:6.5
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:0
Rotatable Bond Count:2
Exact Mass:234.234750957
Heavy Atom Count:17
Complexity:250

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(C)(C)C1CCC(=CC2CCCCC2)CC1

Technology Process of 1-tert-Butyl-4-(cyclohexylmethylidene)cyclohexane

There total 4 articles about 1-tert-Butyl-4-(cyclohexylmethylidene)cyclohexane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 89657-02-3
(4-tert-Butyl-1-trimethylsilanyl-cyclohexyl)-cyclohexyl-methanol

: 89657-03-4
(4-tert-butylcyclohexylidene)cyclohexylmethane

Guidance literature:: With potassium hydride; In tetrahydrofuran; at 25 ℃; for 1.5h;
DOI:10.1021/ja00323a031

Reference yield:

: 85895-63-2
1,1-bis(phenylthio)-4-tert-butylcyclohexane

: 89657-03-4
(4-tert-butylcyclohexylidene)cyclohexylmethane

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) lithium 1-(dimethylamino)naphthalenide / 1.) THF, 15 min, -78 deg C

2: 1.) lithium 1-(dimethylamino)naphthalenide / 1.) THF, 4 min, -78 deg C; 2.) 15 min

3: 89 percent / KH / tetrahydrofuran / 1.5 h / 25 °C

With lithium 1-(dimethylamino)naphthalenide; potassium hydride; In tetrahydrofuran;
DOI:10.1021/ja00323a031

Reference yield:

: 98-53-3
4-tercbutyl-cyclohexanone

: 89657-03-4
(4-tert-butylcyclohexylidene)cyclohexylmethane

Guidance literature:: Multi-step reaction with 4 steps

1: 84 percent / HCl gas

2: 1.) lithium 1-(dimethylamino)naphthalenide / 1.) THF, 15 min, -78 deg C

3: 1.) lithium 1-(dimethylamino)naphthalenide / 1.) THF, 4 min, -78 deg C; 2.) 15 min

4: 89 percent / KH / tetrahydrofuran / 1.5 h / 25 °C

With hydrogenchloride; lithium 1-(dimethylamino)naphthalenide; potassium hydride; In tetrahydrofuran;
DOI:10.1021/ja00323a031