Ethyl (6-chloropyridin-3-yl)carbamate

Base Information

Chemical Name:Ethyl (6-chloropyridin-3-yl)carbamate
CAS No.:89660-15-1
Molecular Formula:C₈H₉ClN₂O₂
Molecular Weight:200.625
Hs Code.:
DSSTox Substance ID:DTXSID30572467
Wikidata:Q82460829
Mol file:89660-15-1.mol

Synonyms:89660-15-1;Ethyl (6-chloropyridin-3-yl)carbamate;Ethyl (6-Chloro-3-pyridyl)carbamate;ethyl N-(6-chloropyridin-3-yl)carbamate;Carbamic acid, (6-chloro-3-pyridinyl)-, ethyl ester;SCHEMBL7896726;DTXSID30572467;AC7161;MFCD23722377;Ethyl(6-chloropyridin-3-yl)carbamate;AKOS017370389;SY039251;CS-0459329;A917167

Suppliers and Price of Ethyl (6-chloropyridin-3-yl)carbamate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Crysdot
Ethyl(6-chloropyridin-3-yl)carbamate 97%
5g
$ 330.00

AK Scientific
Ethyl(6-chloropyridin-3-yl)carbamate
5g
$ 937.00

Total 5 raw suppliers

Chemical Property of Ethyl (6-chloropyridin-3-yl)carbamate

Chemical Property:

Boiling Point:262.3±25.0 °C(Predicted)
PKA:12.06±0.70(Predicted)
PSA：54.71000
Density:1.332±0.06 g/cm3(Predicted)
LogP:2.31700
XLogP3:1.8
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:3
Exact Mass:200.0352552
Heavy Atom Count:13
Complexity:178

Purity/Quality:

97% ^*data from raw suppliers

Ethyl(6-chloropyridin-3-yl)carbamate 97% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCOC(=O)NC1=CN=C(C=C1)Cl

Technology Process of Ethyl (6-chloropyridin-3-yl)carbamate

There total 1 articles about Ethyl (6-chloropyridin-3-yl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.5%

: 5350-93-6
6-Chloro-pyridin-3-ylamine

: 541-41-3
chloroformic acid ethyl ester

: 89660-15-1
ethyl (2-chloro-5-pyridyl)carbamate

Guidance literature:: In chloroform; for 8h; Heating;

Reference yield: 62.0%

: 89660-15-1
ethyl (2-chloro-5-pyridyl)carbamate

: 89660-16-2
ethyl (6-chloro-2-nitro-3-pyridyl)carbamate

Guidance literature:: With sulfuric acid; nitric acid; at 90 - 95 ℃; for 0.333333h;

Reference yield:

: 89660-15-1
ethyl (2-chloro-5-pyridyl)carbamate

: 89660-24-2
1-methyl-3-phenyl-5-chloroimidazo<4,5-b>pyridin-2-one

Guidance literature:: Multi-step reaction with 5 steps

1: 62 percent / conc. H₂SO₄, 100percent HNO₃ / 0.33 h / 90 - 95 °C

2: K₂CO₃ / acetone / 6 h / Heating

3: 70 percent / 37percent HCl, granulated tin / 0.25 h / Heating

4: 95 percent / EtONa / 6 h / Heating

5: 23 percent / anhydrous AcOK, Cu powder, CuCl / dimethylformamide / 16 h / Heating

With hydrogenchloride; tin; sulfuric acid; nitric acid; sodium ethanolate; potassium acetate; copper; potassium carbonate; copper(l) chloride; In N,N-dimethyl-formamide; acetone;