4-tert-Butyl-1-(methoxymethoxy)cyclohex-1-ene

Base Information

Chemical Name:4-tert-Butyl-1-(methoxymethoxy)cyclohex-1-ene
CAS No.:89726-97-6
Molecular Formula:C12H22O2
Molecular Weight:198.305
Hs Code.:
DSSTox Substance ID:DTXSID50533237

Synonyms:89726-97-6;4-tert-Butyl-1-(methoxymethoxy)cyclohex-1-ene;DTXSID50533237

Suppliers and Price of 4-tert-Butyl-1-(methoxymethoxy)cyclohex-1-ene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-tert-Butyl-1-(methoxymethoxy)cyclohex-1-ene

Chemical Property:

XLogP3:3.4
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:4
Exact Mass:198.161979940
Heavy Atom Count:14
Complexity:201

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(C)(C)C1CCC(=CC1)OCOC

Technology Process of 4-tert-Butyl-1-(methoxymethoxy)cyclohex-1-ene

There total 6 articles about 4-tert-Butyl-1-(methoxymethoxy)cyclohex-1-ene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 109-72-8,29786-93-4
n-butyllithium

: 89726-83-0,89746-17-8
trans-4-tert-butyl-O-(methoxymethyl)-1-(tri-n-butylstannyl)cyclohexanol

: 89726-87-4
trans-4-tert-butyl-O-(methoxymethyl)cyclohexanol

: 89726-90-9
cis-4-tert-butyl-O-(methoxymethyl)cyclohexanol

: 89726-97-6
4-tert-butyl-1-(methoxymethoxy)-1-cyclohexene

Guidance literature:: With n-Butyl chloride; In 1,2-dimethoxyethane; under argon; tin compound in DME cooled to -78 °C; nBuLi added; quench with excess alkyl halide;; poured in NH4Cl-soln./petroleum ether; sepn. of org. layer; dried; concd.; chromd.; NMR;
DOI:10.1021/ja00211a024

Reference yield: 58.0%

: 109-72-8,29786-93-4
n-butyllithium

: 89726-83-0,89746-17-8
trans-4-tert-butyl-O-(methoxymethyl)-1-(tri-n-butylstannyl)cyclohexanol

: 89726-87-4
trans-4-tert-butyl-O-(methoxymethyl)cyclohexanol

: 89726-90-9
cis-4-tert-butyl-O-(methoxymethyl)cyclohexanol

: 98-53-3
4-tercbutyl-cyclohexanone

: 89726-97-6
4-tert-butyl-1-(methoxymethoxy)-1-cyclohexene

Guidance literature:: With 3-chloroprop-1-ene; In 1,2-dimethoxyethane; under argon; tin compound in DME cooled to -78 °C; nBuLi added; quench with excess alkyl halide;; poured in NH4Cl-soln./petroleum ether; sepn. of org. layer; dried; concd.; chromd.; NMR;
DOI:10.1021/ja00211a024