Technology Process of Benzene, 1-(1-chloro-2,2-dimethylpropyl)-4-[2-(4-nitrophenyl)ethenyl]-,
(E)-
There total 5 articles about Benzene, 1-(1-chloro-2,2-dimethylpropyl)-4-[2-(4-nitrophenyl)ethenyl]-,
(E)- which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
thionyl chloride;
for 1h;
Ambient temperature;
DOI:10.1021/ja00323a013
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 84 percent / benzene / Heating
2: 76 percent / NaOMe / methanol / 72 h
3: 94 percent / LiBH4 / ethanol; diethyl ether / 1 h
4: 83 percent / thionyl chloride / 1 h / Ambient temperature
With
lithium borohydride; thionyl chloride; sodium methylate;
In
methanol; diethyl ether; ethanol; benzene;
DOI:10.1021/ja00323a013
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 68 percent / benzoyl peroxide, N-bromosuccinimide / CCl4 / 24 h / Heating
2: 84 percent / benzene / Heating
3: 76 percent / NaOMe / methanol / 72 h
4: 94 percent / LiBH4 / ethanol; diethyl ether / 1 h
5: 83 percent / thionyl chloride / 1 h / Ambient temperature
With
N-Bromosuccinimide; lithium borohydride; thionyl chloride; sodium methylate; dibenzoyl peroxide;
In
methanol; tetrachloromethane; diethyl ether; ethanol; benzene;
DOI:10.1021/ja00323a013
