Trimethyl[(trimethylstannyl)methyl]germane

Base Information

• Chemical Name: Trimethyl[(trimethylstannyl)methyl]germane
• CAS No.: 89748-43-6
• Molecular Formula: C7H20GeSn
• Molecular Weight: 295.536
• DSSTox Substance ID: DTXSID30540585
• Wikidata: Q82416631

Synonyms:89748-43-6;Trimethyl[(trimethylstannyl)methyl]germane;DTXSID30540585

Chemical Property of Trimethyl[(trimethylstannyl)methyl]germane

Chemical Property:

• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 0
• Rotatable Bond Count: 2
• Exact Mass: 297.979881
• Heavy Atom Count: 9
• Complexity: 86.1

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C[Ge](C)(C)C[Sn](C)(C)C

Technology Process of Trimethyl[(trimethylstannyl)methyl]germane

There total 1 articles about Trimethyl[(trimethylstannyl)methyl]germane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 32.0%

trimethylstannylmethyl iodide (23696-40-4) + trimethylbromogermane (1066-37-1) → (CH3)3SnCH2Ge(CH3)3 (89748-43-6) + 1,2-Bis-(trimethylstannyl)-ethan (56580-70-2)

Guidance literature:

With magnesium; In diethyl ether; (N2); a mixture of (CH3)3SnCH2I and Mg in ether refluxed for 1 h; a soln. of (CH3)3GeBr added dropwise over a period of 45 min; refluxed for 1 h and stirred overnight; treated with saturated NH4Cl; distd.;

DOI:10.1021/om00124a003

Reference yield:

(CH3)3SnCH2Ge(CH3)3 (89748-43-6) → Brommethyl-trimethyl-german (88496-91-7) + trimethyltin bromide (1066-44-0)

Guidance literature:

With bromine; In dichloromethane; (N2); monitored by (1)H NMR;

DOI:10.1021/om00124a003

Reference yield:

(CH3)3SnCH2Ge(CH3)3 (89748-43-6) → tetramethylgermane (865-52-1) + trimethyltin acetate (1118-14-5)

Guidance literature:

With acetic acid; In acetic acid; (N2); monitored by (1)H NMR; Kinetics;

DOI:10.1021/om00124a003

upstream raw materials:

trimethylstannylmethyl iodide

trimethylbromogermane

Downstream raw materials:

tetramethylgermane

perfluoroacetoxy-trimethyl-stannane

Brommethyl-trimethyl-german

trimethyltin bromide

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