1,3-Cyclohexanedione, 5-(2,4-dichlorophenyl)-4-methyl-

Base Information

Chemical Name:1,3-Cyclohexanedione, 5-(2,4-dichlorophenyl)-4-methyl-
CAS No.:89756-75-2
Molecular Formula:C13H12Cl2O2
Molecular Weight:271.143
Hs Code.:
DSSTox Substance ID:DTXSID30435760

Synonyms:89756-75-2;1,3-Cyclohexanedione, 5-(2,4-dichlorophenyl)-4-methyl-;DTXSID30435760

Suppliers and Price of 1,3-Cyclohexanedione, 5-(2,4-dichlorophenyl)-4-methyl-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 0 raw suppliers

Chemical Property of 1,3-Cyclohexanedione, 5-(2,4-dichlorophenyl)-4-methyl-

Chemical Property:

XLogP3:3.2
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:1
Exact Mass:270.0214350
Heavy Atom Count:17
Complexity:329

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC1C(CC(=O)CC1=O)C2=C(C=C(C=C2)Cl)Cl

Technology Process of 1,3-Cyclohexanedione, 5-(2,4-dichlorophenyl)-4-methyl-

There total 5 articles about 1,3-Cyclohexanedione, 5-(2,4-dichlorophenyl)-4-methyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 874-42-0
2,4-dichlorobenzaldeyhde

: 89756-75-2
5-(2,4-dichlorophenyl)-4-methyl-1,3-cyclohexanedione

Guidance literature:: Multi-step reaction with 4 steps

1: 67 percent / HCl(gas) / 2 h / 0 °C

2: EtONa / ethanol / 2 h / Heating

3: 2 N aq. NaOH / 2 h / Heating

4: 50percent H₂SO₄ / 2 h / Heating; pH 2

With hydrogenchloride; sodium hydroxide; sulfuric acid; sodium ethanolate; In ethanol;
DOI:10.1021/jm00097a001

Reference yield:

: 66897-02-7
4-(2,4-dichlorophenyl)-3-methyl-3-buten-2-one

: 89756-75-2
5-(2,4-dichlorophenyl)-4-methyl-1,3-cyclohexanedione

Guidance literature:: Multi-step reaction with 3 steps

1: EtONa / ethanol / 2 h / Heating

2: 2 N aq. NaOH / 2 h / Heating

3: 50percent H₂SO₄ / 2 h / Heating; pH 2

With sodium hydroxide; sulfuric acid; sodium ethanolate; In ethanol;
DOI:10.1021/jm00097a001