5-Methyl-2-nitro-N-(piperidin-1-yl)benzamide

Base Information

Chemical Name:5-Methyl-2-nitro-N-(piperidin-1-yl)benzamide
CAS No.:89804-90-0
Molecular Formula:C13H17N3O3
Molecular Weight:263.296
Hs Code.:
DSSTox Substance ID:DTXSID80523565
Wikidata:Q82389741

Synonyms:89804-90-0;5-Methyl-2-nitro-N-(piperidin-1-yl)benzamide;DTXSID80523565

Suppliers and Price of 5-Methyl-2-nitro-N-(piperidin-1-yl)benzamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 0 raw suppliers

Chemical Property of 5-Methyl-2-nitro-N-(piperidin-1-yl)benzamide

Chemical Property:

XLogP3:2.5
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:2
Exact Mass:263.12699141
Heavy Atom Count:19
Complexity:337

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC(=C(C=C1)[N+](=O)[O-])C(=O)NN2CCCCC2

Technology Process of 5-Methyl-2-nitro-N-(piperidin-1-yl)benzamide

There total 3 articles about 5-Methyl-2-nitro-N-(piperidin-1-yl)benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 38818-49-4
5-methyl-2-nitrobenzoyl chloride

: 2213-43-6
1-Aminopiperidine

: 89804-90-0
1-(5-methyl-2-nitrobenzoyl)-2,2-pentamethylenehydrazine

Guidance literature:: In diethyl ether; Ambient temperature; overbight;
DOI:10.1002/jhet.5570200623

Reference yield: 56.0%

: 3113-72-2
5-methyl-2-nitrobenzoic acid

: 2213-43-6
1-Aminopiperidine

: 89804-90-0
1-(5-methyl-2-nitrobenzoyl)-2,2-pentamethylenehydrazine

Guidance literature:: With tetrachlorosilane; In pyridine;
DOI:10.1002/jhet.5570250143

Reference yield:

: 3113-72-2
5-methyl-2-nitrobenzoic acid

: 89804-90-0
1-(5-methyl-2-nitrobenzoyl)-2,2-pentamethylenehydrazine

Guidance literature:: Multi-step reaction with 2 steps

1: SOCl₂ / 7 h / Heating

2: 78 percent / diethyl ether / Ambient temperature; overbight

With thionyl chloride; In diethyl ether;
DOI:10.1002/jhet.5570200623