2-Amino-5-methyl-N-(piperidin-1-yl)benzamide

Base Information

Chemical Name:2-Amino-5-methyl-N-(piperidin-1-yl)benzamide
CAS No.:89804-92-2
Molecular Formula:C13H19N3O
Molecular Weight:233.30900
Hs Code.:
DSSTox Substance ID:DTXSID00523567
Wikidata:Q82389745

Synonyms:89804-92-2;2-Amino-5-methyl-N-(piperidin-1-yl)benzamide;DTXSID00523567;AKOS021332706

Suppliers and Price of 2-Amino-5-methyl-N-(piperidin-1-yl)benzamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 0 raw suppliers

Chemical Property of 2-Amino-5-methyl-N-(piperidin-1-yl)benzamide

Chemical Property:

PSA：61.85000
Density:1.16±0.1 g/cm3(Predicted)
LogP:2.80180
XLogP3:2.5
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:2
Exact Mass:233.152812238
Heavy Atom Count:17
Complexity:263

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC(=C(C=C1)N)C(=O)NN2CCCCC2

Technology Process of 2-Amino-5-methyl-N-(piperidin-1-yl)benzamide

There total 2 articles about 2-Amino-5-methyl-N-(piperidin-1-yl)benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 89804-90-0
1-(5-methyl-2-nitrobenzoyl)-2,2-pentamethylenehydrazine

: 89804-92-2
1-(5-Methyl-2-aminobenzoyl)-2,2-pentamethylenehydrazine

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethanol; low pressure;
DOI:10.1002/jhet.5570200623

Reference yield:

: 3113-72-2
5-methyl-2-nitrobenzoic acid

: 89804-92-2
1-(5-Methyl-2-aminobenzoyl)-2,2-pentamethylenehydrazine

Guidance literature:: Multi-step reaction with 3 steps

1: SOCl₂ / 7 h / Heating

2: 78 percent / diethyl ether / Ambient temperature; overbight

3: 94 percent / H₂ / 5percent Pd/C / ethanol / low pressure

With thionyl chloride; hydrogen; palladium on activated charcoal; In diethyl ether; ethanol;
DOI:10.1002/jhet.5570200623