[3-(Dimethylphosphoryl)propyl](oxo)diphenyl-lambda~5~-phosphane

Base Information

Chemical Name:[3-(Dimethylphosphoryl)propyl](oxo)diphenyl-lambda~5~-phosphane
CAS No.:89807-16-9
Molecular Formula:C₁₇H₂₂O₂P₂
Molecular Weight:320.308
Hs Code.:
DSSTox Substance ID:DTXSID10523255
Nikkaji Number:J2.547.368J
Wikidata:Q82389247

Synonyms:89807-16-9;DTXSID10523255;[3-(Dimethylphosphoryl)propyl](oxo)diphenyl-lambda~5~-phosphane

Suppliers and Price of [3-(Dimethylphosphoryl)propyl](oxo)diphenyl-lambda~5~-phosphane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of [3-(Dimethylphosphoryl)propyl](oxo)diphenyl-lambda~5~-phosphane

Chemical Property:

Melting Point:145-148 °C
Boiling Point:495.5±28.0 °C(Predicted)
PSA：53.76000
Density:1.12±0.1 g/cm3(Predicted)
LogP:4.01330
XLogP3:2
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:6
Exact Mass:320.10950394
Heavy Atom Count:21
Complexity:379

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CP(=O)(C)CCCP(=O)(C1=CC=CC=C1)C2=CC=CC=C2

Technology Process of [3-(Dimethylphosphoryl)propyl](oxo)diphenyl-lambda~5~-phosphane

There total 5 articles about [3-(Dimethylphosphoryl)propyl](oxo)diphenyl-lambda~5~-phosphane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 89807-14-7
<3-(dimethylphenylphosphonio)propyl>triphenylphosphonium dibromide

: 89807-16-9
1-dimethylphosphinoyl-3-diphenylphosphinoylpropane

Guidance literature:: With sodium hydroxide; for 1h; Heating;

Reference yield:

: 7211-39-4
dimethyl phosphine oxide

: 6224-95-9
diphenyl(1-propynyl)phosphine oxide

: 89807-16-9
1-dimethylphosphinoyl-3-diphenylphosphinoylpropane

Guidance literature:: dimethyl phosphine oxide; diphenyl(1-propynyl)phosphine oxide; With tributylphosphine; In isopropyl alcohol; at 150 ℃; for 0.5h; Microwave irradiation;

With palladium 10% on activated carbon; hydrogen; In ethanol; at 20 ℃; for 24h;
DOI:10.1055/s-0029-1217176

Reference yield:

: 3607-17-8
3-bromopropyltriphenylphosphonium bromide

: 89807-16-9
1-dimethylphosphinoyl-3-diphenylphosphinoylpropane

Guidance literature:: Multi-step reaction with 2 steps

1: 94 percent / dimethylformamide / 4 h / Heating

2: 92 percent / 20percent aqueous sodium hydroxide / 1 h / Heating

With sodium hydroxide; In N,N-dimethyl-formamide;