1,2-Bis(3-fluoro-4-methoxyphenyl)disulfane

Base Information

Chemical Name:1,2-Bis(3-fluoro-4-methoxyphenyl)disulfane
CAS No.:89818-28-0
Molecular Formula:C14H12F2O2S2
Molecular Weight:314.377
Hs Code.:
DSSTox Substance ID:DTXSID60531047
Wikidata:Q82402604

Synonyms:1,2-bis(3-fluoro-4-methoxyphenyl)disulfane;89818-28-0;Disulfide, bis(3-fluoro-4-methoxyphenyl);DTXSID60531047;MFCD33022457;BS-48383;E75520;1,1'-Disulfanediylbis(3-fluoro-4-methoxybenzene);2-FLUORO-4-[(3-FLUORO-4-METHOXYPHENYL)DISULFANYL]-1-METHOXYBENZENE

Suppliers and Price of 1,2-Bis(3-fluoro-4-methoxyphenyl)disulfane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Ambeed
1,2-Bis(3-fluoro-4-methoxyphenyl)disulfane 97%
5g
$ 515.00

Ambeed
1,2-Bis(3-fluoro-4-methoxyphenyl)disulfane 97%
1g
$ 179.00

Ambeed
1,2-Bis(3-fluoro-4-methoxyphenyl)disulfane 97%
250mg
$ 93.00

Ambeed
1,2-Bis(3-fluoro-4-methoxyphenyl)disulfane 97%
100mg
$ 64.00

Total 5 raw suppliers

Chemical Property of 1,2-Bis(3-fluoro-4-methoxyphenyl)disulfane

Chemical Property:

PSA：69.06000
LogP:4.78140
XLogP3:4.2
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:6
Rotatable Bond Count:5
Exact Mass:314.02467829
Heavy Atom Count:20
Complexity:268

Purity/Quality:

97% ^*data from raw suppliers

1,2-Bis(3-fluoro-4-methoxyphenyl)disulfane 97% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1=C(C=C(C=C1)SSC2=CC(=C(C=C2)OC)F)F

Technology Process of 1,2-Bis(3-fluoro-4-methoxyphenyl)disulfane

There total 4 articles about 1,2-Bis(3-fluoro-4-methoxyphenyl)disulfane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 179899-07-1
4-fluoro-2-methoxyphenylboronic acid

: 89818-28-0
1,2-bis(3-fluoro-4-methoxyphenyl)disulfane

Guidance literature:: With CrPOM; sodium thiosulfate; In water; toluene; at 100 ℃; for 24h;
DOI:10.1039/d1gc01415c

Reference yield:

: 89818-27-9
3-fluoro-4-methoxybenzenethiol

: 89818-28-0
1,2-bis(3-fluoro-4-methoxyphenyl)disulfane

Guidance literature:: With sodium hydroxide; iodine; In ethanol;
DOI:10.1002/jhet.5570200651

Reference yield:

: 321-28-8
1-fluoro-2-methoxybenzene

: 89818-28-0
1,2-bis(3-fluoro-4-methoxyphenyl)disulfane

Guidance literature:: Multi-step reaction with 3 steps

1: 77 percent / acetic acid; acetic anhydride / 7 h / Ambient temperature

2: 93 percent / LAH / diethyl ether / 2 h / Heating

3: 4M NaOH, iodine / ethanol

With sodium hydroxide; lithium aluminium tetrahydride; iodine; In diethyl ether; ethanol; acetic anhydride; acetic acid;
DOI:10.1002/jhet.5570200651