Benzenamine, N-[1-[4-(trifluoromethyl)phenyl]ethylidene]-

Base Information

Chemical Name:Benzenamine, N-[1-[4-(trifluoromethyl)phenyl]ethylidene]-
CAS No.:898282-29-6
Molecular Formula:C15H12F3N
Molecular Weight:263.262
Hs Code.:
DSSTox Substance ID:DTXSID80461690
Nikkaji Number:J2.061.546J

Synonyms:Benzenamine, N-[1-[4-(trifluoromethyl)phenyl]ethylidene]-;898282-29-6;SCHEMBL13819189;DTXSID80461690;FSNVUIDWCYKPAV-UHFFFAOYSA-N;FSNVUIDWCYKPAV-YBFXNURJSA-N

Suppliers and Price of Benzenamine, N-[1-[4-(trifluoromethyl)phenyl]ethylidene]-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Benzenamine, N-[1-[4-(trifluoromethyl)phenyl]ethylidene]-

Chemical Property:

XLogP3:4.3
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:2
Exact Mass:263.09218387
Heavy Atom Count:19
Complexity:308

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(=NC1=CC=CC=C1)C2=CC=C(C=C2)C(F)(F)F

Technology Process of Benzenamine, N-[1-[4-(trifluoromethyl)phenyl]ethylidene]-

There total 5 articles about Benzenamine, N-[1-[4-(trifluoromethyl)phenyl]ethylidene]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

: 705-31-7
4-trifluoromethylphenylacetylene

: 62-53-3
aniline

: 898282-29-6
N-(1-(4-(trifluoromethyl)phenyl)ethylidene)aniline

Guidance literature:: With silver trifluoromethanesulfonate; In 1,4-dioxane; at 70 ℃; for 5h; Inert atmosphere;
DOI:10.1021/acs.inorgchem.1c02070

Reference yield: 40.0%

: 709-63-7
1-(4-trifluoromethylphenyl)ethanone

: 62-53-3
aniline

: 898282-29-6
N-(1-(4-(trifluoromethyl)phenyl)ethylidene)aniline

Guidance literature:: With montmorillonite K₁₀ Clay; In toluene; at 130 ℃; for 4.5h; Microwave irradiation;
DOI:10.3762/bjoc.9.71

Reference yield:

: 86767-33-1
1-phenyl-1-<4'-(trifluoromethyl)phenyl>ethanol

: 1-phenyl-N-(4-(trifluoromethyl)phenyl)ethan-1-imine

: 898282-29-6
N-(1-(4-(trifluoromethyl)phenyl)ethylidene)aniline

Guidance literature:: Multi-step reaction with 3 steps

1: sodium azide; trifluoroacetic acid / dichloromethane / -5 - 0 °C / Inert atmosphere

2: lithium aluminium tetrahydride / diethyl ether / 3 h / 0 - 20 °C / Inert atmosphere

3: caesium carbonate; iodine / tetrachloromethane; 1,2-dichloro-ethane / Reflux

With lithium aluminium tetrahydride; sodium azide; iodine; caesium carbonate; trifluoroacetic acid; In tetrachloromethane; diethyl ether; dichloromethane; 1,2-dichloro-ethane;
DOI:10.1039/d1nj02932k