2-(2-Cyclohexylideneethyl)-2-ethyl-1,3-dioxolane

Base Information

Chemical Name:2-(2-Cyclohexylideneethyl)-2-ethyl-1,3-dioxolane
CAS No.:89839-78-1
Molecular Formula:C13H22O2
Molecular Weight:210.31300
Hs Code.:
DSSTox Substance ID:DTXSID00527909

Synonyms:89839-78-1;2-(2-Cyclohexylideneethyl)-2-ethyl-1,3-dioxolane;DTXSID00527909

Suppliers and Price of 2-(2-Cyclohexylideneethyl)-2-ethyl-1,3-dioxolane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
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Total 0 raw suppliers

Chemical Property of 2-(2-Cyclohexylideneethyl)-2-ethyl-1,3-dioxolane

Chemical Property:

PSA：18.46000
LogP:3.42010
XLogP3:3.1
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:3
Exact Mass:210.161979940
Heavy Atom Count:15
Complexity:219

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCC1(OCCO1)CC=C2CCCCC2

Technology Process of 2-(2-Cyclohexylideneethyl)-2-ethyl-1,3-dioxolane

There total 5 articles about 2-(2-Cyclohexylideneethyl)-2-ethyl-1,3-dioxolane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 89839-64-5
5-diphenylphosphinoyl-5-(1-hydroxycyclohexyl)pentan-3-one ethylene acetal

: 89839-78-1
1-(cyclohexylidene)pentan-3-one ethylene acetal

Guidance literature:: With sodium hydride; In tetrahydrofuran; for 1h; Heating;

Reference yield:

: 108-94-1,11119-77-0,9003-41-2,9075-99-4
cyclohexanone

: 89839-78-1
1-(cyclohexylidene)pentan-3-one ethylene acetal

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) BuLi / 1.) THF, -78 deg C, 10 min, 2.) -78 deg C -> room temperature

2: 83 percent / NaH / tetrahydrofuran / 1 h / Heating

With n-butyllithium; sodium hydride; In tetrahydrofuran;

Reference yield:

: 69803-57-2
1-diphenylphosphinoylpentan-3-one

: 89839-78-1
1-(cyclohexylidene)pentan-3-one ethylene acetal

Guidance literature:: Multi-step reaction with 3 steps

1: 88 percent / TsOH / benzene / 24 h / Heating

2: 1.) BuLi / 1.) THF, -78 deg C, 10 min, 2.) -78 deg C -> room temperature

3: 83 percent / NaH / tetrahydrofuran / 1 h / Heating

With n-butyllithium; sodium hydride; toluene-4-sulfonic acid; In tetrahydrofuran; benzene;