[2-(2-Ethyl-1,3-dioxolan-2-yl)ethyl](oxo)diphenyl-lambda~5~-phosphane

Base Information

Chemical Name:[2-(2-Ethyl-1,3-dioxolan-2-yl)ethyl](oxo)diphenyl-lambda~5~-phosphane
CAS No.:69803-68-5
Molecular Formula:C19H23O3P
Molecular Weight:330.364
Hs Code.:
DSSTox Substance ID:DTXSID40527903

Synonyms:69803-68-5;DTXSID40527903;[2-(2-Ethyl-1,3-dioxolan-2-yl)ethyl](oxo)diphenyl-lambda~5~-phosphane

Suppliers and Price of [2-(2-Ethyl-1,3-dioxolan-2-yl)ethyl](oxo)diphenyl-lambda~5~-phosphane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of [2-(2-Ethyl-1,3-dioxolan-2-yl)ethyl](oxo)diphenyl-lambda~5~-phosphane

Chemical Property:

XLogP3:3.2
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:6
Exact Mass:330.13848159
Heavy Atom Count:23
Complexity:383

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCC1(OCCO1)CCP(=O)(C2=CC=CC=C2)C3=CC=CC=C3

Technology Process of [2-(2-Ethyl-1,3-dioxolan-2-yl)ethyl](oxo)diphenyl-lambda~5~-phosphane

There total 2 articles about [2-(2-Ethyl-1,3-dioxolan-2-yl)ethyl](oxo)diphenyl-lambda~5~-phosphane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 107-21-1
ethylene glycol

: 69803-57-2
1-diphenylphosphinoylpentan-3-one

: 69803-68-5
1-diphenylphosphinoylpentan-3-one ethylene acetal

Guidance literature:: With toluene-4-sulfonic acid; In benzene; for 24h; Heating;

Reference yield: 12.0%

: 89839-63-4
5-diphenylphosphinoyl-6-ethyl-6-hydroxyoctan-3-one ethylene acetal

: 89839-77-0
6-ethyloct-5-en-3-one ethylene acetal

: 69803-68-5
1-diphenylphosphinoylpentan-3-one ethylene acetal

Guidance literature:: With sodium hydride; In tetrahydrofuran; for 1h; Heating;

Reference yield:

: 69803-68-5
1-diphenylphosphinoylpentan-3-one ethylene acetal

: 89839-78-1
1-(cyclohexylidene)pentan-3-one ethylene acetal

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) BuLi / 1.) THF, -78 deg C, 10 min, 2.) -78 deg C -> room temperature

2: 83 percent / NaH / tetrahydrofuran / 1 h / Heating

With n-butyllithium; sodium hydride; In tetrahydrofuran;