2-(4-Nitrophenyl)-1,3-dioxan-5-ol

Base Information

• Chemical Name: 2-(4-Nitrophenyl)-1,3-dioxan-5-ol
• CAS No.: 89863-03-6
• Molecular Formula: C10H11NO5
• Molecular Weight: 225.201
• DSSTox Substance ID: DTXSID10515478
• Nikkaji Number: J3.147.970C

Synonyms:2-(4-Nitrophenyl)-1,3-dioxan-5-ol;89863-03-6;DTXSID10515478

Chemical Property of 2-(4-Nitrophenyl)-1,3-dioxan-5-ol

Chemical Property:

• XLogP3: 0.5
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 5
• Rotatable Bond Count: 1
• Exact Mass: 225.06372245
• Heavy Atom Count: 16
• Complexity: 238

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1C(COC(O1)C2=CC=C(C=C2)[N+](=O)[O-])O

Technology Process of 2-(4-Nitrophenyl)-1,3-dioxan-5-ol

There total 4 articles about 2-(4-Nitrophenyl)-1,3-dioxan-5-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

4-nitrobenzaldehdye (555-16-8) + glycerol (56-81-5,25618-55-7,64333-26-2,8013-25-0) → 2-p-nitrophenyl-5-hydroxy-1,3-dioxane (89863-03-6)

Guidance literature:

With toluene-4-sulfonic acid; In toluene; azeotropic removing of water;

Reference yield:

4-nitrobenzaldehdye (555-16-8) + glycerol (56-81-5,25618-55-7,64333-26-2,8013-25-0) → 2-p-nitrophenyl-5-hydroxy-1,3-dioxane (89863-03-6)

Guidance literature:

With sulfuric acid; at 120 ℃; unter vermindertem Druck;

Reference yield:

4-nitrobenzaldehdye (555-16-8) + glycerol (56-81-5,25618-55-7,64333-26-2,8013-25-0) → [2-(4-nitro-phenyl)-[1,3]dioxolan-4-yl]-methanol (448234-93-3) + 2-p-nitrophenyl-5-hydroxy-1,3-dioxane (89863-03-6)

Guidance literature:

With WO₃ loaded on boehmite; In toluene; at 100 ℃; for 20h;

DOI:10.1039/d1nj04860k

upstream raw materials:

4-nitrobenzaldehdye

glycerol

Downstream raw materials:

2-p-nitrophenyl-1,3-dioxan-5-yl p-aminobenzoate

4-{[1-(4-Nonyloxy-phenyl)-meth-(E)-ylidene]-amino}-benzoic acid 2-(4-nitro-phenyl)-[1,3]dioxan-5-yl ester

4-{[1-(4-Octyloxy-phenyl)-meth-(E)-ylidene]-amino}-benzoic acid 2-(4-nitro-phenyl)-[1,3]dioxan-5-yl ester

4-{[1-(4-Heptyloxy-phenyl)-meth-(E)-ylidene]-amino}-benzoic acid 2-(4-nitro-phenyl)-[1,3]dioxan-5-yl ester

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