1-(Bromomethyl)-2-(2-nitrophenoxy)benzene

Base Information

Chemical Name:1-(Bromomethyl)-2-(2-nitrophenoxy)benzene
CAS No.:89914-07-8
Molecular Formula:C₁₃H₁₀BrNO₃
Molecular Weight:308.131
Hs Code.:
DSSTox Substance ID:DTXSID20522037
Wikidata:Q82386959

Synonyms:1-(Bromomethyl)-2-(2-nitrophenoxy)benzene;89914-07-8;DTXSID20522037

Suppliers and Price of 1-(Bromomethyl)-2-(2-nitrophenoxy)benzene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-(Bromomethyl)-2-(2-nitrophenoxy)benzene

Chemical Property:

XLogP3:3.8
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:3
Exact Mass:306.98441
Heavy Atom Count:18
Complexity:282

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C(=C1)CBr)OC2=CC=CC=C2[N+](=O)[O-]

Technology Process of 1-(Bromomethyl)-2-(2-nitrophenoxy)benzene

There total 1 articles about 1-(Bromomethyl)-2-(2-nitrophenoxy)benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.8%

: 54106-40-0
1-methyl-2-(2-nitrophenoxy)benzene

: 89914-07-8
2-bromomethyl-2'-nitrodiphenyl ether

Guidance literature:: With N-Bromosuccinimide; pentachlorobenzoyl chloride; In tetrachloromethane; for 30h; Heating;

Reference yield: 25.0%

: 89914-07-8
2-bromomethyl-2'-nitrodiphenyl ether

: 18522-92-4
sodium p-toluenesulfonamide

: 89914-12-5
4-Methyl-N,N-bis-[2-(2-nitro-phenoxy)-benzyl]-benzenesulfonamide

Guidance literature:: In N,N-dimethyl-formamide; at 110 ℃; for 10h;

Reference yield:

: 89914-07-8
2-bromomethyl-2'-nitrodiphenyl ether

: tetrabenzo--tetrahydro-1,9-dioxo-5,12,14-triazocyclohexadecane

Guidance literature:: Multi-step reaction with 4 steps

1: 25 percent / dimethylformamide / 10 h / 110 °C

2: 37 percent / H₂ / PtO₂ / methanol / 30 °C / 7600 Torr

3: 97 percent / pyridine

4: 1.) sodium n-butanolate / 1.) butanol, reflux, 30 min., 2.) DMF, 80-90 deg, 10 h

With pyridine; hydrogen; sodium butanolate; platinum(IV) oxide; In methanol; N,N-dimethyl-formamide;