2-(2-Methylanilino)-4H-pyrido[3,2-e][1,3]selenazin-4-one

Base Information

Chemical Name:2-(2-Methylanilino)-4H-pyrido[3,2-e][1,3]selenazin-4-one
CAS No.:89927-24-2
Molecular Formula:C₁₄H₁₁N₃OSe
Molecular Weight:316.221
Hs Code.:
DSSTox Substance ID:DTXSID90529775
Wikidata:Q82400451

Synonyms:89927-24-2;DTXSID90529775;2-(2-Methylanilino)-4H-pyrido[3,2-e][1,3]selenazin-4-one

Suppliers and Price of 2-(2-Methylanilino)-4H-pyrido[3,2-e][1,3]selenazin-4-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemical Property of 2-(2-Methylanilino)-4H-pyrido[3,2-e][1,3]selenazin-4-one

Chemical Property:

Melting Point:216-218 °C
Boiling Point:481.9±47.0 °C(Predicted)
PSA：58.11000
LogP:1.52090
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:2
Exact Mass:317.00673
Heavy Atom Count:19
Complexity:385

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC=CC=C1NC2=NC(=O)C3=C([Se]2)N=CC=C3

Technology Process of 2-(2-Methylanilino)-4H-pyrido[3,2-e][1,3]selenazin-4-one

There total 3 articles about 2-(2-Methylanilino)-4H-pyrido[3,2-e][1,3]selenazin-4-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

: 89914-54-5
1-(2-Chloro-pyridine-3-carbonyl)-3-o-tolyl-selenourea

: 89927-24-2
2-[(E)-o-Tolylimino]-2,3-dihydro-pyrido[3,2-e][1,3]selenazin-4-one

Guidance literature:: With lithium hydride; In N,N-dimethyl-formamide; 1. 20 degC 2. 50-60 deg C;

Reference yield:

: 49609-84-9
2-Chloronicotinoyl chloride

: 89927-24-2
2-[(E)-o-Tolylimino]-2,3-dihydro-pyrido[3,2-e][1,3]selenazin-4-one

Guidance literature:: Multi-step reaction with 3 steps

1: acetone / 0.08 h / 0 - 5 °C / in a nitrogen atmosphere

2: 24 percent / acetone / 0.17 h / under nitrogen

3: 52 percent / lithium hydride / dimethylformamide / 1. 20 degC 2. 50-60 deg C

With lithium hydride; In N,N-dimethyl-formamide; acetone;

Reference yield:

: 89914-71-6
2-chloronicotinoyl isoselenocyanate

: 89927-24-2
2-[(E)-o-Tolylimino]-2,3-dihydro-pyrido[3,2-e][1,3]selenazin-4-one

Guidance literature:: Multi-step reaction with 2 steps

1: 24 percent / acetone / 0.17 h / under nitrogen

2: 52 percent / lithium hydride / dimethylformamide / 1. 20 degC 2. 50-60 deg C

With lithium hydride; In N,N-dimethyl-formamide; acetone;