Ethanone, 1-(2-phenyl-4-pyrimidinyl)-, oxime

Base Information

Chemical Name:Ethanone, 1-(2-phenyl-4-pyrimidinyl)-, oxime
CAS No.:89967-09-9
Molecular Formula:C12H11N3O
Molecular Weight:213.239
Hs Code.:

Synonyms:

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Chemical Property of Ethanone, 1-(2-phenyl-4-pyrimidinyl)-, oxime

Chemical Property:

Purity/Quality:

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MSDS Files:: SDS file from LookChem

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Technology Process of Ethanone, 1-(2-phenyl-4-pyrimidinyl)-, oxime

There total 5 articles about Ethanone, 1-(2-phenyl-4-pyrimidinyl)-, oxime which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 89967-03-3
4-ethyl-2-phenyl-pyrimidine

: 89967-09-9
1-(2-Phenyl-pyrimidin-4-yl)-ethanone oxime

Guidance literature:: With hydrogenchloride; n-propyl nitrite; In ethanol; for 2h; Ambient temperature;

Reference yield:

: 1670-14-0
benzamidine monohydrochloride

: 89967-09-9
1-(2-Phenyl-pyrimidin-4-yl)-ethanone oxime

Guidance literature:: Multi-step reaction with 4 steps

1: 88 percent / 1.) sodium methoxide / 1.) methanol, rt., 12 h; 2.) 120 deg C, 20 mmHg, 2 h

2: 85 percent / phosphoryl chloride / 3 h / Heating

3: 96 percent / hydrogen/conc. ammonia / 5percent palladium charcoal / methanol

4: 92 percent / propyl nitrite, HCl / ethanol / 2 h / Ambient temperature

With hydrogenchloride; ammonium hydroxide; n-propyl nitrite; hydrogen; sodium methylate; trichlorophosphate; palladium on activated charcoal; In methanol; ethanol;

Reference yield:

: 83501-10-4
6-ethyl-2-phenyl-4(3H)-pyrimidinone

: 89967-09-9
1-(2-Phenyl-pyrimidin-4-yl)-ethanone oxime

Guidance literature:: Multi-step reaction with 3 steps

1: 85 percent / phosphoryl chloride / 3 h / Heating

2: 96 percent / hydrogen/conc. ammonia / 5percent palladium charcoal / methanol

3: 92 percent / propyl nitrite, HCl / ethanol / 2 h / Ambient temperature

With hydrogenchloride; ammonium hydroxide; n-propyl nitrite; hydrogen; trichlorophosphate; palladium on activated charcoal; In methanol; ethanol;