Benzenemethanamine, N-methyl-N-phenyl-, hydrochloride

Base Information

Chemical Name:Benzenemethanamine, N-methyl-N-phenyl-, hydrochloride
CAS No.:90097-08-8
Molecular Formula:C14H15N.ClH
Molecular Weight:233.741
Hs Code.:

Synonyms:

Suppliers and Price of Benzenemethanamine, N-methyl-N-phenyl-, hydrochloride

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 3 raw suppliers

Chemical Property of Benzenemethanamine, N-methyl-N-phenyl-, hydrochloride

Chemical Property:

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Benzenemethanamine, N-methyl-N-phenyl-, hydrochloride

There total 3 articles about Benzenemethanamine, N-methyl-N-phenyl-, hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 1934-92-5
N-methyl-N-phenyl-benzamide

: 90097-08-8
N-methyl-N-benzylaniline hydrochloride

Guidance literature:: N-methyl-N-phenyl-benzamide; With [κ²-{Ph₂P(Se)NC₉H₆N}Al(Me)₂]; 4,4,5,5-tetramethyl-[1,3,2]-dioxaboralane; at 20 ℃; for 12h; Schlenk technique; Glovebox;

With hydrogenchloride; In water; chemoselective reaction;
DOI:10.1039/c9dt01806a

Reference yield:

: C₁₄H₁₃ClN⁽¹⁺⁾*Cl^(1-)

: 90097-08-8
N-methyl-N-benzylaniline hydrochloride

Guidance literature:: With hydrogen; tris(2,6-difluorophenyl)borane triethylphosphine oxide; In chloroform; at 40 ℃; for 48h; under 60006 Torr; Autoclave;
DOI:10.1021/jacs.8b12997

Reference yield:

: 93-98-1,5705-51-1
N-phenyl benzoyl amide

: 90097-08-8
N-methyl-N-benzylaniline hydrochloride

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydride / tetrahydrofuran; mineral oil / 0 °C / Inert atmosphere

1.2: 2 h / 0 - 20 °C / Inert atmosphere

2.1: tris(2,6-difluorophenyl)borane triethylphosphine oxide; oxalyl dichloride / chloroform / Sealed tube; Inert atmosphere; Glovebox

3.1: hydrogen; tris(2,6-difluorophenyl)borane triethylphosphine oxide / chloroform / 48 h / 40 °C / 60006 Torr / Autoclave

With oxalyl dichloride; hydrogen; sodium hydride; tris(2,6-difluorophenyl)borane triethylphosphine oxide; In tetrahydrofuran; chloroform; mineral oil;
DOI:10.1021/jacs.8b12997