Phosphine, diphenyl[3-(trimethylstannyl)propyl]-

Base Information

Chemical Name:Phosphine, diphenyl[3-(trimethylstannyl)propyl]-
CAS No.:90127-33-6
Molecular Formula:C₁₈H₂₅PSn
Molecular Weight:391.08
Hs Code.:

Synonyms:

Suppliers and Price of Phosphine, diphenyl[3-(trimethylstannyl)propyl]-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of Phosphine, diphenyl[3-(trimethylstannyl)propyl]-

Chemical Property:

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Phosphine, diphenyl[3-(trimethylstannyl)propyl]-

There total 2 articles about Phosphine, diphenyl[3-(trimethylstannyl)propyl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 1631-73-8
trimethylstannane

: 2741-38-0
allyldiphenylphosphine

: 90127-33-6
3-diphenylphosphinopropyltrimethylstannane

Guidance literature:: With 2,2'-azobis(isobutyronitrile); H.Weichmann, G. Quell and A. Tzschach, Z. Anorg. Allg. Chem., 462(1980)7; H. Weichmann, C. Muegge, A. Grand und J. B. Robert, J. Organomet. Chem., 238(1982) 343; H. P. Abicht, C. Muegge und H. Weichmann, Z. Anorg. Allg. Chem, 467(1980) 203; elem. anal.;
DOI:10.1016/S0022-328X(00)99156-3

Reference yield:

: 16643-09-7
trimethylstannyl sodium

: 90127-33-6
3-diphenylphosphinopropyltrimethylstannane

Guidance literature:: With 3-chloropropyldiphenylphosphine; In diethyl ether; ammonia; byproducts: NaCl; NH3 soln. of NaSnMe3 at ca -70°C was added dropwise to Et2O soln. of Cl(CH2)2PPh2, evapg., treatment with Et2O, filtration; evapg., distn. in vac.; elem. anal.;
DOI:10.1016/S0022-328X(00)99156-3

Reference yield: 83.0%

: 90127-33-6
3-diphenylphosphinopropyltrimethylstannane

: 1066-45-1
trimethyltin(IV)chloride

: 90127-39-2
3-diphenylphosphinopropyl-dimethylzinnchlorid

Guidance literature:: In neat (no solvent); byproducts: Me4Sn; heating of the react. mixt. at ca 60°C, then 1-2 d at room temp., treatment with hexane, filtration, evapg. of filtrate, adding of Me3SnCl, repeating of procedure; crystn. from benzene/hexane or ppn. with H2O from EtOH soln.; elem. anal.;
DOI:10.1016/S0022-328X(00)99156-3