Technology Process of Benzene, [[1-(iodomethyl)-2-methylpropoxy]methyl]-, (R)-
There total 5 articles about Benzene, [[1-(iodomethyl)-2-methylpropoxy]methyl]-, (R)- which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
triphenyl phosphite; methyl iodide;
In
diethyl ether;
for 5h;
Heating;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 40 percent / sodium nitrite / aq. H2SO4 / 2 h / 0 °C
2: 76 percent / conc. H2SO4 / methanol / 3 h / Heating
3: 41 percent / NaH / tetrahydrofuran / 4 h / Ambient temperature
4: 89 percent / LiAlH4 / diethyl ether / Ambient temperature
5: 56 percent / methyl iodide, triphenylphosphite / diethyl ether / 5 h / Heating
With
triphenyl phosphite; lithium aluminium tetrahydride; sulfuric acid; sodium hydride; sodium nitrite; methyl iodide;
In
tetrahydrofuran; methanol; diethyl ether; sulfuric acid;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 76 percent / conc. H2SO4 / methanol / 3 h / Heating
2: 41 percent / NaH / tetrahydrofuran / 4 h / Ambient temperature
3: 89 percent / LiAlH4 / diethyl ether / Ambient temperature
4: 56 percent / methyl iodide, triphenylphosphite / diethyl ether / 5 h / Heating
With
triphenyl phosphite; lithium aluminium tetrahydride; sulfuric acid; sodium hydride; methyl iodide;
In
tetrahydrofuran; methanol; diethyl ether;
