Benzene, [[1-(iodomethyl)-2-methylpropoxy]methyl]-, (R)-

Base Information

Chemical Name:Benzene, [[1-(iodomethyl)-2-methylpropoxy]methyl]-, (R)-
CAS No.:90211-84-0
Molecular Formula:C₁₂H₁₇IO
Molecular Weight:304.171
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Benzene, [[1-(iodomethyl)-2-methylpropoxy]methyl]-, (R)-

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Benzene, [[1-(iodomethyl)-2-methylpropoxy]methyl]-, (R)-

There total 5 articles about Benzene, [[1-(iodomethyl)-2-methylpropoxy]methyl]-, (R)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: 84994-63-8
(R)-2-benzyloxy-3-methyl-1-butanol

: 90211-84-0
(2R)-benzyloxy-3-methyl-1-iodobutane

Guidance literature:: With triphenyl phosphite; methyl iodide; In diethyl ether; for 5h; Heating;

Reference yield:

: 640-68-6,25609-85-2,7004-03-7,921-10-8
D-Val-OH

: 90211-84-0
(2R)-benzyloxy-3-methyl-1-iodobutane

Guidance literature:: Multi-step reaction with 5 steps

1: 40 percent / sodium nitrite / aq. H₂SO₄ / 2 h / 0 °C

2: 76 percent / conc. H₂SO₄ / methanol / 3 h / Heating

3: 41 percent / NaH / tetrahydrofuran / 4 h / Ambient temperature

4: 89 percent / LiAlH₄ / diethyl ether / Ambient temperature

5: 56 percent / methyl iodide, triphenylphosphite / diethyl ether / 5 h / Heating

With triphenyl phosphite; lithium aluminium tetrahydride; sulfuric acid; sodium hydride; sodium nitrite; methyl iodide; In tetrahydrofuran; methanol; diethyl ether; sulfuric acid;

Reference yield:

: 17407-56-6
(R)-2-Hydroxy-3-methylbutyric acid

: 90211-84-0
(2R)-benzyloxy-3-methyl-1-iodobutane

Guidance literature:: Multi-step reaction with 4 steps

1: 76 percent / conc. H₂SO₄ / methanol / 3 h / Heating

2: 41 percent / NaH / tetrahydrofuran / 4 h / Ambient temperature

3: 89 percent / LiAlH₄ / diethyl ether / Ambient temperature

4: 56 percent / methyl iodide, triphenylphosphite / diethyl ether / 5 h / Heating

With triphenyl phosphite; lithium aluminium tetrahydride; sulfuric acid; sodium hydride; methyl iodide; In tetrahydrofuran; methanol; diethyl ether;