1,2-Bis(dipropylacetamido)-1,2-di-4-pyridylethane

Base Information

Chemical Name:1,2-Bis(dipropylacetamido)-1,2-di-4-pyridylethane
CAS No.:77502-23-9
Molecular Formula:C₂₈H₄₂N₄O₂
Molecular Weight:466.667
Hs Code.:2933399090
DSSTox Substance ID:DTXSID70998687
Mol file:77502-23-9.mol

Synonyms:77502-23-9;1,2-Bis(dipropylacetamido)-1,2-di-4-pyridylethane;N,N'-(1,2-Di-4-pyridinyl-1,2-ethanediyl)bis(2-propylpentanamide);Pentanamide, N,N'-(1,2-di-4-pyridinyl-1,2-ethanediyl)bis(2-propyl-;DTXSID70998687;C28H42N4O2;C28-H42-N4-O2;LS-101504;N,N'-[1,2-Di(pyridin-4-yl)ethane-1,2-diyl]bis(2-propylpentanimidic acid)

Suppliers and Price of 1,2-Bis(dipropylacetamido)-1,2-di-4-pyridylethane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
1,2-BIS(DIPROPYLACETAMIDO)-1,2-DI-4-PYRIDYLETHANE 95.00%
5MG
$ 502.37

Total 2 raw suppliers

Chemical Property of 1,2-Bis(dipropylacetamido)-1,2-di-4-pyridylethane

Chemical Property:

Boiling Point:695.4oC at 760 mmHg
Flash Point:374.4oC
PSA：90.96000
Density:1.042g/cm3
LogP:7.60480
XLogP3:5.5
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:15
Exact Mass:466.33077660
Heavy Atom Count:34
Complexity:511

Purity/Quality:

99% ^*data from raw suppliers

1,2-BIS(DIPROPYLACETAMIDO)-1,2-DI-4-PYRIDYLETHANE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCCC(CCC)C(=O)NC(C1=CC=NC=C1)C(C2=CC=NC=C2)NC(=O)C(CCC)CCC

Technology Process of 1,2-Bis(dipropylacetamido)-1,2-di-4-pyridylethane

There total 5 articles about 1,2-Bis(dipropylacetamido)-1,2-di-4-pyridylethane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 56427-39-5
N-(4-picolyl)-dipropylacetamid

: 77502-40-0
2-Propyl-pentanoic acid (1-oxy-pyridin-4-ylmethyl)-amide

: 77502-23-9
2-Propyl-pentanoic acid [2-(2-propyl-pentanoylamino)-1,2-di-pyridin-4-yl-ethyl]-amide

Guidance literature:: With acetic anhydride; at 70 ℃; for 3h;
DOI:10.1002/jhet.5570200658

Reference yield: 43.0%

: 77502-40-0
2-Propyl-pentanoic acid (1-oxy-pyridin-4-ylmethyl)-amide

: 77502-23-9
2-Propyl-pentanoic acid [2-(2-propyl-pentanoylamino)-1,2-di-pyridin-4-yl-ethyl]-amide

Guidance literature:: In acetic anhydride; at 140 ℃; for 1.5h;
DOI:10.1002/jhet.5570180707

Reference yield:

: 3731-53-1
4-(aminomethyl)pyridine

: 77502-23-9
2-Propyl-pentanoic acid [2-(2-propyl-pentanoylamino)-1,2-di-pyridin-4-yl-ethyl]-amide

Guidance literature:: Multi-step reaction with 3 steps

1: dicyclohexylcarbodiimide / acetonitrile / 24 h / Ambient temperature

2: 60 percent / hydrogen peroxide (40 percent) / acetic acid / 80 °C

3: 43 percent / acetic anhydride / 1.5 h / 140 °C

With dihydrogen peroxide; dicyclohexyl-carbodiimide; In acetic anhydride; acetic acid; acetonitrile;
DOI:10.1002/jhet.5570180707