4-broMo-1-Methoxy-2-(Methylsulfonyl)benzene

Base Information

Chemical Name:4-broMo-1-Methoxy-2-(Methylsulfonyl)benzene
CAS No.:90531-99-0
Molecular Formula:C8H9BrO3S
Molecular Weight:265.128
Hs Code.:2909309090
Mol file:90531-99-0.mol

Synonyms:Benzene,4-bromo-1-methoxy-2-(methylsulfonyl);4-bromo-2-methanesulfonyl-1-methoxybenzene;Methyl-(5-brom-2-methoxy-phenyl)-sulfon;4-bromo-1-methoxy-2-(methylsulfonyl)benzene;

Suppliers and Price of 4-broMo-1-Methoxy-2-(Methylsulfonyl)benzene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
4-Bromo-2-methanesulfonyl-1-methoxybenzene
250mg
$ 380.00

Crysdot
4-Bromo-1-methoxy-2-(methylsulfonyl)benzene 97%
1g
$ 518.00

Total 5 raw suppliers

Chemical Property of 4-broMo-1-Methoxy-2-(Methylsulfonyl)benzene

Chemical Property:

Melting Point:91-92 °C(Solv: benzene (71-43-2); ligroine (8032-32-4))
Boiling Point:408.3±45.0 °C(Predicted)
PSA：51.75000
Density:1.546±0.06 g/cm3(Predicted)
LogP:2.94200

Purity/Quality:

97% ^*data from raw suppliers

4-Bromo-2-methanesulfonyl-1-methoxybenzene ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 4-broMo-1-Methoxy-2-(Methylsulfonyl)benzene

There total 6 articles about 4-broMo-1-Methoxy-2-(Methylsulfonyl)benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 23095-05-8
5-bromo-2-methoxybenzenesulfonyl chloride

: 74-88-4
methyl iodide

: 90531-99-0
4-bromo-1-methoxy-2-(methylsulfonyl)benzene

Guidance literature:: 5-bromo-2-methoxybenzenesulfonyl chloride; With sodium hydrogencarbonate; sodium sulfite; In 1,4-dioxane; water; at 70 ℃; for 1h;

methyl iodide; In N,N-dimethyl-formamide; for 2h;
DOI:10.1021/ml200163b

Reference yield: 69.0%

: 23095-05-8
5-bromo-2-methoxybenzenesulfonyl chloride

: 77-78-1
dimethyl sulfate

: 90531-99-0
4-bromo-1-methoxy-2-(methylsulfonyl)benzene

Guidance literature:: 5-bromo-2-methoxybenzenesulfonyl chloride; With sodium hydrogencarbonate; sodium sulfite; In water; at 20 - 80 ℃; for 22h;

dimethyl sulfate; With sodium hydrogencarbonate; In water; at 120 ℃; for 8h;

Reference yield: 40.0%

: 3-bromo-4-methyl-1-(methylsulfonyl)benzene

: 74-88-4
methyl iodide

: 90531-99-0
4-bromo-1-methoxy-2-(methylsulfonyl)benzene

Guidance literature:: 3-bromo-4-methyl-1-(methylsulfonyl)benzene; With sodium hydride; In N,N-dimethyl-formamide; mineral oil; at 20 ℃; for 0.5h;

methyl iodide; In N,N-dimethyl-formamide; mineral oil; at 20 ℃; for 3h;