Propanedioyl dichloride, [(2-methoxyphenyl)hydrazono]-

Base Information

• Chemical Name: Propanedioyl dichloride, [(2-methoxyphenyl)hydrazono]-
• CAS No.: 90800-12-7
• Molecular Formula: C₁₀H₈Cl₂N₂O₃
• Molecular Weight: 275.091
• Mol file: 90800-12-7.mol

Synonyms:

Chemical Property of Propanedioyl dichloride, [(2-methoxyphenyl)hydrazono]-

Chemical Property:

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Propanedioyl dichloride, [(2-methoxyphenyl)hydrazono]-

There total 3 articles about Propanedioyl dichloride, [(2-methoxyphenyl)hydrazono]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(2-methoxy-phenylhydrazono)-malonic acid (91818-58-5) → (2-methoxy-phenylhydrazono)-malonyl chloride (90800-12-7)

Guidance literature:

With thionyl chloride;

DOI:10.1039/jr9610002828

Reference yield:

2-methoxyaniline hydrochloride (134-29-2) → (2-methoxy-phenylhydrazono)-malonyl chloride (90800-12-7)

Guidance literature:

Multi-step reaction with 3 steps

1: (i) NaNO₂, (ii) /BRN= 774687/, aq. NaOAc

2: aq. NaOH

3: SOCl₂

With sodium hydroxide; thionyl chloride;

DOI:10.1039/jr9610002828

Reference yield:

(2-methoxy-phenylhydrazono)-malonic acid diethyl ester (13636-66-3) → (2-methoxy-phenylhydrazono)-malonyl chloride (90800-12-7)

Guidance literature:

Multi-step reaction with 2 steps

1: aq. NaOH

2: SOCl₂

With sodium hydroxide; thionyl chloride;

DOI:10.1039/jr9610002828

upstream raw materials:

(2-methoxy-phenylhydrazono)-malonic acid

2-methoxyaniline hydrochloride

(2-methoxy-phenylhydrazono)-malonic acid diethyl ester

Downstream raw materials:

8-methoxy-1H-cinnolin-4-one