Technology Process of 2H-Indol-2-one, 1,3-dihydro-3-phenyl-3-(phenylamino)-
There total 9 articles about 2H-Indol-2-one, 1,3-dihydro-3-phenyl-3-(phenylamino)- which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
caesium carbonate;
In
dichloromethane;
at 25 ℃;
for 15h;
DOI:10.1021/ol061191z
- Guidance literature:
-
Multi-step reaction with 2 steps
1: sodium hydrogencarbonate / toluene / 24 h / 80 °C / Molecular sieve; Inert atmosphere; Sealed tube
2: tetrakis(acetonitrile)palladium(II) bis(tetrafluoroborate); 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; triethylamine / 24 h / 100 °C / Inert atmosphere; Sealed tube
With
tetrakis(acetonitrile)palladium(II) bis(tetrafluoroborate); sodium hydrogencarbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; triethylamine;
In
toluene;
DOI:10.1021/ol302119j
DOI:10.1021/ol302119j
- Guidance literature:
-
Multi-step reaction with 3 steps
1: pyridine / dichloromethane / 2 h / 0 - 20 °C / Inert atmosphere
2: sodium hydrogencarbonate / toluene / 24 h / 80 °C / Molecular sieve; Inert atmosphere; Sealed tube
3: tetrakis(acetonitrile)palladium(II) bis(tetrafluoroborate); 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; triethylamine / 24 h / 100 °C / Inert atmosphere; Sealed tube
With
pyridine; tetrakis(acetonitrile)palladium(II) bis(tetrafluoroborate); sodium hydrogencarbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; triethylamine;
In
dichloromethane; toluene;
DOI:10.1021/ol302119j
DOI:10.1021/ol302119j