2-Methoxy-4,5-dimethylbenzoic acid

Base Information

Chemical Name:2-Methoxy-4,5-dimethylbenzoic acid
CAS No.:91061-36-8
Molecular Formula:C10H12O3
Molecular Weight:180.203
Hs Code.:
DSSTox Substance ID:DTXSID30577270
Wikidata:Q82467226
Mol file:91061-36-8.mol

Synonyms:2-Methoxy-4,5-dimethylbenzoic acid;91061-36-8;2-methoxy-4,5-dimethyl-benzoic acid;Benzoic acid, 2-methoxy-4,5-dimethyl-;DTXSID30577270;2-Methoxy-4,5-dimethylbenzoicacid;AMY28086;MFCD14538071;AKOS005151367;SB73990;AS-61850;CS-0168204;W17034;EN300-2001552;A928322

Suppliers and Price of 2-Methoxy-4,5-dimethylbenzoic acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

AOBChem
2-Methoxy-4,5-dimethylbenzoicacid 97%
500mg
$ 187.00

Total 13 raw suppliers

Chemical Property of 2-Methoxy-4,5-dimethylbenzoic acid

Chemical Property:

Melting Point:141-142 °C
Boiling Point:328.6±37.0 °C(Predicted)
PKA:4.33±0.10(Predicted)
Density:1.136±0.06 g/cm3(Predicted)
XLogP3:2.1
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:2
Exact Mass:180.078644241
Heavy Atom Count:13
Complexity:191

Purity/Quality:

97% ^*data from raw suppliers

2-Methoxy-4,5-dimethylbenzoicacid 97% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC(=C(C=C1C)OC)C(=O)O

Technology Process of 2-Methoxy-4,5-dimethylbenzoic acid

There total 11 articles about 2-Methoxy-4,5-dimethylbenzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 124-38-9,18923-20-1
carbon dioxide

: 33500-88-8
1-bromo-2-methoxy-4,5-dimethylbenzene

: 91061-36-8
2-methoxy-4,5-dimethylbenzoic acid

Guidance literature:: 1-bromo-2-methoxy-4,5-dimethylbenzene; With n-butyllithium; In tetrahydrofuran; hexane; at -70 ℃; for 2h;

carbon dioxide; In hexane; at -50 ℃; for 2.5h;

Reference yield:

: 4685-47-6
3,4-dimethylanisole

: 91061-36-8
2-methoxy-4,5-dimethylbenzoic acid

Guidance literature:: Multi-step reaction with 2 steps

1.1: bromine / dichloromethane / 1 h / -70 °C

2.1: n-butyllithium / tetrahydrofuran; hexane / 2 h / -70 °C

2.2: 2.5 h / -50 °C

With n-butyllithium; bromine; In tetrahydrofuran; hexane; dichloromethane;