1-Pyrrolidinecarboxylic acid, 3-[[[4-ethyl-3-(3-methoxypropoxy)benzoyl](1-methylethyl)amino]methyl]-4 -formyl-, 1,1-dimethylethyl ester, (3R,4S)-

Base Information

Chemical Name:1-Pyrrolidinecarboxylic acid, 3-[[[4-ethyl-3-(3-methoxypropoxy)benzoyl](1-methylethyl)amino]methyl]-4 -formyl-, 1,1-dimethylethyl ester, (3R,4S)-
CAS No.:911114-09-5
Molecular Formula:C27H42N2O6
Molecular Weight:490.64
Hs Code.:

1-Pyrrolidinecarboxylic acid,
3-[[[4-ethyl-3-(3-methoxypropoxy)benzoyl](1-methylethyl)amino]methyl]-4
-formyl-, 1,1-dimethylethyl ester, (3R,4S)-

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-Pyrrolidinecarboxylic acid, 3-[[[4-ethyl-3-(3-methoxypropoxy)benzoyl](1-methylethyl)amino]methyl]-4 -formyl-, 1,1-dimethylethyl ester, (3R,4S)-

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Technology Process of 1-Pyrrolidinecarboxylic acid, 3-[[[4-ethyl-3-(3-methoxypropoxy)benzoyl](1-methylethyl)amino]methyl]-4 -formyl-, 1,1-dimethylethyl ester, (3R,4S)-

There total 1 articles about 1-Pyrrolidinecarboxylic acid, 3-[[[4-ethyl-3-(3-methoxypropoxy)benzoyl](1-methylethyl)amino]methyl]-4 -formyl-, 1,1-dimethylethyl ester, (3R,4S)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 911114-09-5
(3R,4S)-3-({[4-ethyl-3-(3-methoxy-propoxy)-benzoyl]-isopropyl-amino}-methyl)-4-formyl-pyrrolidine-1-carboxylic acid tert-butyl ester

Guidance literature:

Reference yield:

: 911114-09-5
(3R,4S)-3-({[4-ethyl-3-(3-methoxy-propoxy)-benzoyl]-isopropyl-amino}-methyl)-4-formyl-pyrrolidine-1-carboxylic acid tert-butyl ester

: 765-30-0
Cyclopropylamine

: 911114-15-3
(3R,4R)-3-cyclopropylaminomethyl-4-({[4-ethyl-3-(3-methoxy-propoxy)-benzoyl]-isopropyl-amino}-methyl)-pyrrolidine-1-carboxylic acid tert-butyl ester

Guidance literature:: With sodium tris(acetoxy)borohydride; In 1,1-dichloroethane; at 20 ℃;

Reference yield:

: 911114-09-5
(3R,4S)-3-({[4-ethyl-3-(3-methoxy-propoxy)-benzoyl]-isopropyl-amino}-methyl)-4-formyl-pyrrolidine-1-carboxylic acid tert-butyl ester

: cyclopropyl-[(3S,4S)-4-({[4-ethyl-3-(3-methoxy-propoxy)-benzoyl]-isopropyl-amino}-methyl)-pyrrolidin-3-ylmethyl]-carbamic acid isobutyl ester hydrochloride

Guidance literature:: Multi-step reaction with 3 steps

1: sodium tris(acetoxy)borohydride / 1,1-dichloroethane / 20 °C

2: triethylamine / dichloromethane / 20 °C

3: hydrogenchloride / 1,4-dioxane

With hydrogenchloride; sodium tris(acetoxy)borohydride; triethylamine; In 1,4-dioxane; 1,1-dichloroethane; dichloromethane;