3-Pyridinecarbonyl azide, 6-methyl-

Base Information

Chemical Name:3-Pyridinecarbonyl azide, 6-methyl-
CAS No.:64038-04-6
Molecular Formula:C7H6 N4 O
Molecular Weight:162.151
Hs Code.:2933399090
DSSTox Substance ID:DTXSID50214059
Nikkaji Number:J78.916J
Wikidata:Q83089791

Synonyms:64038-04-6;Nicotinoyl azide, 6-methyl-;3-Pyridinecarbonyl azide, 6-methyl-;6-methylpyridine-3-carbonyl azide;SCHEMBL21767215;DTXSID50214059;6-Methyl-3-pyridinecarbonyl azide;AHA100139;LS-130402

Suppliers and Price of 3-Pyridinecarbonyl azide, 6-methyl-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of 3-Pyridinecarbonyl azide, 6-methyl-

Chemical Property:

Boiling Point:°Cat760mmHg
Flash Point:°C
PSA：79.71000
Density:g/cm³
LogP:1.29326
XLogP3:2.1
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:1
Exact Mass:162.05416083
Heavy Atom Count:12
Complexity:221

Purity/Quality:: 95% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=NC=C(C=C1)C(=O)N=[N+]=[N-]

Technology Process of 3-Pyridinecarbonyl azide, 6-methyl-

There total 4 articles about 3-Pyridinecarbonyl azide, 6-methyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 51598-76-6
6-methyl-nicotinoyl chloride

: 64038-04-6
6-methyl-nicotinoyl azide

Guidance literature:: With sodium azide; triethylamine; In acetonitrile; at 5 ℃; for 0.666667h;
DOI:10.1021/jm050293c

Reference yield:

: 6-methylnicotinic acid hydrochloride

: 64038-04-6
6-methyl-nicotinoyl azide

Guidance literature:: Multi-step reaction with 2 steps

1: (COCl)2; DMF / CH₂Cl₂

2: sodium azide; Et₃N / acetonitrile / 0.67 h / 5 °C

With sodium azide; oxalyl dichloride; triethylamine; N,N-dimethyl-formamide; In dichloromethane; acetonitrile;
DOI:10.1021/jm050293c

Reference yield:

: 21684-59-3
ethyl 6-methylnicotinate

: 64038-04-6
6-methyl-nicotinoyl azide

Guidance literature:: Multi-step reaction with 2 steps

1: N₂H₄+H₂O

2: KNO₂; aqueous HCl

With hydrogenchloride; potassium nitrite; hydrazine hydrate;