(S)-2-N-CBZ-AMINOMETHYL-PYRROLIDINE

Base Information

• Chemical Name: (S)-2-N-CBZ-AMINOMETHYL-PYRROLIDINE
• CAS No.: 913614-65-0
• Molecular Formula: C13H18N2O2
• Molecular Weight: 234.298
• Hs Code.: 2933990090
• Mol file: 913614-65-0.mol

Synonyms:Benzyl N-[[(2S)-pyrrolidin-2-yl]methyl]carbamate;(S)-Pyrrolidin-2-ylmethyl-carbamic acid benzyl ester;

Chemical Property of (S)-2-N-CBZ-AMINOMETHYL-PYRROLIDINE

Chemical Property:

• Vapor Pressure: 1.85E-06mmHg at 25°C
• Refractive Index: 1.531
• Boiling Point: 395.3 °C at 760 mmHg
• Flash Point: 192.9 °C
• PSA: 50.36000
• Density: 1.106 g/cm³
• LogP: 2.38450
• Storage Temp.: 2-8°C

Purity/Quality:

97% ^*data from raw suppliers

(S)-2-N-Cbz-Aminomethyl-pyrrolidine 95+% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of (S)-2-N-CBZ-AMINOMETHYL-PYRROLIDINE

There total 1 articles about (S)-2-N-CBZ-AMINOMETHYL-PYRROLIDINE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1,1-dimethylethyl (2S)-2-[({[(phenylmethyl)oxy]carbonyl}amino)methyl]-1-pyrrolidinecarboxylate (929048-08-8) → phenylmethyl [(2S)-2-pyrrolidinylmethyl]carbamate (913614-65-0)

Guidance literature:

With hydrogenchloride; In 1,4-dioxane; at 20 ℃; for 14h;

Reference yield: 61.0%

phenylmethyl [(2S)-2-pyrrolidinylmethyl]carbamate (913614-65-0) + Diethyl 2-bromomalonate (685-87-0) → diethyl {(2S)-2-[({[(phenylmethyl)oxy]carbonyl}amino)methyl]-1-pyrrolidinyl}propanedioate (929048-09-9)

Guidance literature:

With potassium carbonate; In acetonitrile; at 0 - 20 ℃; for 4h;

Reference yield:

phenylmethyl [(2S)-2-pyrrolidinylmethyl]carbamate (913614-65-0) + cyclohexanecarbaldehyde (2043-61-0) → C20H30N2O2 (1246637-52-4)

Guidance literature:

With sodium cyanoborohydride; acetic acid; In methanol; at 0 - 20 ℃;

upstream raw materials:

1,1-dimethylethyl (2S)-2-[({[(phenylmethyl)oxy]carbonyl}amino)methyl]-1-pyrrolidinecarboxylate

Downstream raw materials:

C₁₇H₂₄N₂O₂

C₂₁H₃₂N₂O₂

C₂₀H₃₀N₂O₂

diethyl {(2S)-2-[({[(phenylmethyl)oxy]carbonyl}amino)methyl]-1-pyrrolidinyl}propanedioate

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