3-Chloro-2,6-diphenylpyridine

Base Information

• Chemical Name: 3-Chloro-2,6-diphenylpyridine
• CAS No.: 91404-09-0
• Molecular Formula: C17H12ClN
• Molecular Weight: 265.742
• DSSTox Substance ID: DTXSID90351876
• Wikidata: Q82128678
• Mol file: 91404-09-0.mol

Synonyms:3-chloro-2,6-diphenylpyridine;91404-09-0;SCHEMBL23277217;DTXSID90351876;STK771234;AKOS001746439

Chemical Property of 3-Chloro-2,6-diphenylpyridine

Chemical Property:

• XLogP3: 4.8
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 2
• Exact Mass: 265.0658271
• Heavy Atom Count: 19
• Complexity: 268

Purity/Quality:

98%,99%, ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC=C(C=C1)C2=NC(=C(C=C2)Cl)C3=CC=CC=C3

Technology Process of 3-Chloro-2,6-diphenylpyridine

There total 2 articles about 3-Chloro-2,6-diphenylpyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

1,5-diphenyl-2,4-dichloropentane-1,5-dione (91404-07-8) → 2,6-diphenyl-3-chloropyridine (91404-09-0)

Guidance literature:

With ammonium acetate; In acetic acid; at 60 - 80 ℃; for 3h;

DOI:10.1007/BF00506668

Reference yield: 34.0%

1,5-diphenyl-2,4-dichloropentane-1,5-dione (91404-07-8) → phenyl(5-phenyl-1H-pyrrol-2-yl)methanone (56900-73-3) + 2,6-diphenyl-3-chloropyridine (91404-09-0)

Guidance literature:

With ammonium acetate; In 1,4-dioxane; at 60 ℃; for 22h; Mechanism; Product distribution; other reagents and solv., var. 2,4-dichloro-1,3-pentanediones;

DOI:10.1007/BF00472290

upstream raw materials:

1,5-diphenyl-2,4-dichloropentane-1,5-dione