1,2-Hydrazinedicarboxylic acid, 1-[[3-(bromomethyl)-8-fluoro-2-phenyl-4-quinolinyl]carbonyl]-2-phenyl-, 1-(1,1-dimethylethyl) 2-methyl ester

Base Information

Chemical Name:1,2-Hydrazinedicarboxylic acid, 1-[[3-(bromomethyl)-8-fluoro-2-phenyl-4-quinolinyl]carbonyl]-2-phenyl-, 1-(1,1-dimethylethyl) 2-methyl ester
CAS No.:914654-43-6
Molecular Formula:C₃₀H₂₇BrFN₃O₅
Molecular Weight:608.464
Hs Code.:

1,2-Hydrazinedicarboxylic acid,
1-[[3-(bromomethyl)-8-fluoro-2-phenyl-4-quinolinyl]carbonyl]-2-phenyl-,
1-(1,1-dimethylethyl) 2-methyl ester

Synonyms:

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Chemical Property of 1,2-Hydrazinedicarboxylic acid, 1-[[3-(bromomethyl)-8-fluoro-2-phenyl-4-quinolinyl]carbonyl]-2-phenyl-, 1-(1,1-dimethylethyl) 2-methyl ester

Chemical Property:

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Technology Process of 1,2-Hydrazinedicarboxylic acid, 1-[[3-(bromomethyl)-8-fluoro-2-phenyl-4-quinolinyl]carbonyl]-2-phenyl-, 1-(1,1-dimethylethyl) 2-methyl ester

There total 4 articles about 1,2-Hydrazinedicarboxylic acid, 1-[[3-(bromomethyl)-8-fluoro-2-phenyl-4-quinolinyl]carbonyl]-2-phenyl-, 1-(1,1-dimethylethyl) 2-methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 914654-42-5
2-(1,1-dimethylethyl) 1-methyl 2-[(8-fluoro-3-methyl-2-phenylquinolin-4-yl)carbonyl]-1-phenylhydrazinedicarboxylate

: 914654-43-6
2-(1,1-dimethylethyl) 1-methyl 2-{[8-fluoro-3-(bromomethyl)-2-phenylquinolin-4-yl]carbonyl}-1-phenylhydrazinedicarboxylate

Guidance literature:: With N-Bromosuccinimide; In tetrachloromethane; Irradiation;
DOI:10.1016/j.bmcl.2006.08.085

Reference yield:

: 914654-41-4
methyl 2-[(8-fluoro-3-methyl-2-phenylquinolin-4-yl)carbonyl]-1-phenylhydrazinecarboxylate

: 914654-43-6
2-(1,1-dimethylethyl) 1-methyl 2-{[8-fluoro-3-(bromomethyl)-2-phenylquinolin-4-yl]carbonyl}-1-phenylhydrazinedicarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: NaH / tetrahydrofuran

2: NBS / CCl₄ / Irradiation

With N-Bromosuccinimide; sodium hydride; In tetrahydrofuran; tetrachloromethane;
DOI:10.1016/j.bmcl.2006.08.085

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 914654-43-6
2-(1,1-dimethylethyl) 1-methyl 2-{[8-fluoro-3-(bromomethyl)-2-phenylquinolin-4-yl]carbonyl}-1-phenylhydrazinedicarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: NaH / tetrahydrofuran

2: NBS / CCl₄ / Irradiation

With N-Bromosuccinimide; sodium hydride; In tetrahydrofuran; tetrachloromethane;
DOI:10.1016/j.bmcl.2006.08.085