Benzene, 1,3-dibromo-5-[[tris(1-methylethyl)silyl]oxy]-

Base Information

Chemical Name:Benzene, 1,3-dibromo-5-[[tris(1-methylethyl)silyl]oxy]-
CAS No.:915411-64-2
Molecular Formula:C15H24Br2OSi
Molecular Weight:408.248
Hs Code.:

Synonyms:

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Chemical Property of Benzene, 1,3-dibromo-5-[[tris(1-methylethyl)silyl]oxy]-

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Technology Process of Benzene, 1,3-dibromo-5-[[tris(1-methylethyl)silyl]oxy]-

There total 4 articles about Benzene, 1,3-dibromo-5-[[tris(1-methylethyl)silyl]oxy]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 13154-24-0
triisopropylsilyl chloride

: 626-41-5
3,5-dibromophenol

: 915411-64-2
(3,5-dibromophenoxy)triisopropylsilane

Guidance literature:: 3,5-dibromophenol; With sodium hydride; In N,N-dimethyl-formamide; mineral oil; at 0 ℃; for 0.5h; Inert atmosphere;

triisopropylsilyl chloride; In N,N-dimethyl-formamide; mineral oil; at 0 - 20 ℃; for 20h; Inert atmosphere;
DOI:10.1021/jm100659v

Reference yield: 100.0%

: 13154-24-0
triisopropylsilyl chloride

: 915411-64-2
(3,5-dibromophenoxy)triisopropylsilane

Guidance literature:: 3,5-dibromoanisole; With sodium hydride; In N,N-dimethyl-formamide; at 0 ℃; for 0.25h;

triisopropylsilyl chloride; In N,N-dimethyl-formamide; at 20 ℃; for 20.25h;

Reference yield:

: 827-94-1
2,6-dibromo-4-nitroaniline

: 915411-64-2
(3,5-dibromophenoxy)triisopropylsilane

Guidance literature:: Multi-step reaction with 4 steps

1.1: sulfuric acid; sodium nitrite / ethanol; water / 3.25 h / Heating / reflux

1.2: 0 °C

2.1: potassium hydroxide; tetrabutylammomium bromide; tetramethylurea / 24.25 h / 20 °C

3.1: tetrabutylammomium bromide; hydrogen bromide / water / 72 h / Heating / reflux

4.1: sodium hydride / N,N-dimethyl-formamide / 0.5 h / 0 °C

4.2: 20 h / 0 - 20 °C

With potassium hydroxide; sulfuric acid; tetrabutylammomium bromide; hydrogen bromide; sodium hydride; tetramethylurea; sodium nitrite; In ethanol; water; N,N-dimethyl-formamide;