Ethanethioamide, N-[2-(3,4-dimethoxyphenyl)ethyl]-

Base Information

Chemical Name:Ethanethioamide, N-[2-(3,4-dimethoxyphenyl)ethyl]-
CAS No.:91564-56-6
Molecular Formula:C12H17NO2S
Molecular Weight:239.338
Hs Code.:
DSSTox Substance ID:DTXSID50442138
Nikkaji Number:J978.290G
Wikidata:Q82259249

Synonyms:91564-56-6;Ethanethioamide, N-[2-(3,4-dimethoxyphenyl)ethyl]-;DTXSID50442138;N-(3,4-Dimethoxyphenethyl)thioacetamide

Suppliers and Price of Ethanethioamide, N-[2-(3,4-dimethoxyphenyl)ethyl]-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Ethanethioamide, N-[2-(3,4-dimethoxyphenyl)ethyl]-

Chemical Property:

XLogP3:1.6
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:5
Exact Mass:239.09799996
Heavy Atom Count:16
Complexity:223

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(=S)NCCC1=CC(=C(C=C1)OC)OC

Technology Process of Ethanethioamide, N-[2-(3,4-dimethoxyphenyl)ethyl]-

There total 5 articles about Ethanethioamide, N-[2-(3,4-dimethoxyphenyl)ethyl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 6275-29-2
N-[2-(3,4-dimethoxyphenyl)ethyl]acetamide

: 91564-56-6
N-thioacetyl-β-(3,4-dimethoxyphenyl)-ethylamine

Guidance literature:: With Lawessons reagent; In toluene; for 2h; Heating;

Reference yield:

: 120-20-7
2-(3,4-dimethoxyphenyl)-ethylamine

: 91564-56-6
N-thioacetyl-β-(3,4-dimethoxyphenyl)-ethylamine

Guidance literature:: Multi-step reaction with 2 steps

1: 96 percent / Et₃N, DMAP / CH₂Cl₂ / Ambient temperature

2: 92 percent / 2,4-bis(4-methoxyphenyl)-1,3-dithia-2,4-diphosphetane-2,4-disulfide / toluene / 2 h / Heating

With Lawessons reagent; dmap; triethylamine; In dichloromethane; toluene;

Reference yield:

: 67616-16-4
N-[2-(3,4-dimethoxyphenyl)ethyl]benzamide

: 91564-56-6
N-thioacetyl-β-(3,4-dimethoxyphenyl)-ethylamine

Guidance literature:: Multi-step reaction with 3 steps

1: 60 percent / Et₃N, DMAP / CH₂Cl₂ / Heating

2: 95 percent / n-BuLi / tetrahydrofuran; hexane / a) 0 deg C, 75 min, b) RT, overnight

3: 92 percent / 2,4-bis(4-methoxyphenyl)-1,3-dithia-2,4-diphosphetane-2,4-disulfide / toluene / 2 h / Heating

With Lawessons reagent; dmap; n-butyllithium; triethylamine; In tetrahydrofuran; hexane; dichloromethane; toluene;