3-Methyl-2-phenylthiazolidine

Base Information

• Chemical Name: 3-Methyl-2-phenylthiazolidine
• CAS No.: 7739-01-7
• Molecular Formula: C10H13NS
• Molecular Weight: 179.28
• Mol file: 7739-01-7.mol

Synonyms:3-methyl-2-phenyl-thiazolidine;Methyl-3-phenyl-thiazolidin;Thiazolidine,3-methyl-2-phenyl;3-Methyl-2-phenyl-thiazolidin;2-phenyl-3-methylthiazolidine-1,3;

Chemical Property of 3-Methyl-2-phenylthiazolidine

Chemical Property:

• Vapor Pressure: 0.00633mmHg at 25°C
• Boiling Point: 271.8°C at 760 mmHg
• Flash Point: 118.2°C
• PSA: 28.54000
• Density: 1.096g/cm³
• LogP: 2.30170

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3-Methyl-2-phenylthiazolidine

There total 3 articles about 3-Methyl-2-phenylthiazolidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.6%

2-(methylamino)ethanethiol (10061-40-2) + benzaldehyde (100-52-7) → 2-phenyl-3-methylthiazolidine-1,3 (7739-01-7)

Guidance literature:

In benzene; for 6h; Heating;

Reference yield: 25.0%

2-phenyl-3-methyl-Δ2-thiazolidinium iodide (26851-78-5) → 2-phenyl-3-methylthiazolidine-1,3 (7739-01-7)

Guidance literature:

With sodium cyanoborohydride; In acetonitrile; at -5 ℃; for 3h;

DOI:10.1016/S0040-4020(01)81096-6

Reference yield:

→ 2-phenyl-3-methylthiazolidine-1,3 (7739-01-7)

Guidance literature:

Phenylthiazolidin I, CH3I;

upstream raw materials:

2-(methylamino)ethanethiol

benzaldehyde

2-phenyl-3-methyl-Δ²-thiazolidinium iodide

Refernces

• 1、 Witek, Stanislaw,Bielawska, Alicja,Bielawski, Jacek. "NEW PESTICIDES AND INTERMEDIATES. PART VIII. QUATERNARY AMMONIUM SALTS OF AZACYCLIC DERIVATIVES". . p. 207 - 212. Retrieved 2007/10/02.