Guanosine, 2'-deoxy-5'-O-[(1,1-dimethylethyl)[(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10- heptadecafluorodecyl)oxy]phenylsilyl]-N-(2-methyl-1-oxopropyl)-

Base Information

Chemical Name:Guanosine, 2'-deoxy-5'-O-[(1,1-dimethylethyl)[(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10- heptadecafluorodecyl)oxy]phenylsilyl]-N-(2-methyl-1-oxopropyl)-
CAS No.:917495-81-9
Molecular Formula:C34H36F17N5O6Si
Molecular Weight:961.748
Hs Code.:

Guanosine,
2'-deoxy-5'-O-[(1,1-dimethylethyl)[(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-
heptadecafluorodecyl)oxy]phenylsilyl]-N-(2-methyl-1-oxopropyl)-

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Guanosine, 2'-deoxy-5'-O-[(1,1-dimethylethyl)[(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10- heptadecafluorodecyl)oxy]phenylsilyl]-N-(2-methyl-1-oxopropyl)-

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MSDS Files:: SDS file from LookChem

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Technology Process of Guanosine, 2'-deoxy-5'-O-[(1,1-dimethylethyl)[(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10- heptadecafluorodecyl)oxy]phenylsilyl]-N-(2-methyl-1-oxopropyl)-

There total 4 articles about Guanosine, 2'-deoxy-5'-O-[(1,1-dimethylethyl)[(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10- heptadecafluorodecyl)oxy]phenylsilyl]-N-(2-methyl-1-oxopropyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 68892-42-2
N-isobutyryl-2'-deoxyguanosine

: 243645-01-4
tert-butyl-phenyl-1H,1H,2H,2H-heptadecafluorodecyloxysilyl bromide

: 917495-81-9
N-(9-{5-[tert-butyl-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluoro-decyloxy)-phenyl-silanyloxymethyl]-4-hydroxy-tetrahydro-furan-2-yl}-6-oxo-6,9-dihydro-1H-purin-2-yl)-isobutyramide

Guidance literature:: With dmap; In dichloromethane; at 20 ℃;
DOI:10.1246/cl.2006.1184

Reference yield:

: 678-39-7
3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluoro-1-decanol

: 917495-81-9
N-(9-{5-[tert-butyl-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluoro-decyloxy)-phenyl-silanyloxymethyl]-4-hydroxy-tetrahydro-furan-2-yl}-6-oxo-6,9-dihydro-1H-purin-2-yl)-isobutyramide

Guidance literature:: Multi-step reaction with 3 steps

1: 88 percent / DMAP; imidazole / CH₂Cl₂ / 20 °C

2: 71 percent / bromine / 1,2-dichloro-ethane / 0 - 20 °C

3: 94 percent / DMAP / CH₂Cl₂ / 20 °C

With 1H-imidazole; dmap; bromine; In dichloromethane; 1,2-dichloro-ethane;
DOI:10.1246/cl.2006.1184

Reference yield:

: 58479-61-1
tert-butylchlorodiphenylsilane

: 917495-81-9
N-(9-{5-[tert-butyl-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluoro-decyloxy)-phenyl-silanyloxymethyl]-4-hydroxy-tetrahydro-furan-2-yl}-6-oxo-6,9-dihydro-1H-purin-2-yl)-isobutyramide

Guidance literature:: Multi-step reaction with 3 steps

1: 88 percent / DMAP; imidazole / CH₂Cl₂ / 20 °C

2: 71 percent / bromine / 1,2-dichloro-ethane / 0 - 20 °C

3: 94 percent / DMAP / CH₂Cl₂ / 20 °C

With 1H-imidazole; dmap; bromine; In dichloromethane; 1,2-dichloro-ethane;
DOI:10.1246/cl.2006.1184