2H-Benzimidazol-2-one, 1,3-dihydro-6-chloro-1-(2,6-dimethylphenyl)-

Base Information

Chemical Name:2H-Benzimidazol-2-one, 1,3-dihydro-6-chloro-1-(2,6-dimethylphenyl)-
CAS No.:79759-78-7
Molecular Formula:C15H13ClN2O
Molecular Weight:272.7295
Hs Code.:
DSSTox Substance ID:DTXSID80229898
Wikidata:Q83110270

Synonyms:BRN 5567680;2H-Benzimidazol-2-one, 1,3-dihydro-6-chloro-1-(2,6-dimethylphenyl)-;79759-78-7;1,3-Dihydro-6-chloro-1-(2,6-dimethylphenyl)-2H-benzimidazol-2-one;DTXSID80229898;LS-33305

Suppliers and Price of 2H-Benzimidazol-2-one, 1,3-dihydro-6-chloro-1-(2,6-dimethylphenyl)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 2H-Benzimidazol-2-one, 1,3-dihydro-6-chloro-1-(2,6-dimethylphenyl)-

Chemical Property:

Boiling Point:°Cat760mmHg
Flash Point:°C
Density:1.293g/cm³
XLogP3:3.7
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:1
Exact Mass:272.0716407
Heavy Atom Count:19
Complexity:352

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=C(C(=CC=C1)C)N2C3=C(C=CC(=C3)Cl)NC2=O

Technology Process of 2H-Benzimidazol-2-one, 1,3-dihydro-6-chloro-1-(2,6-dimethylphenyl)-

There total 5 articles about 2H-Benzimidazol-2-one, 1,3-dihydro-6-chloro-1-(2,6-dimethylphenyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 79759-25-4
[4-Chloro-2-(2,6-dimethyl-phenylamino)-phenyl]-carbamic acid ethyl ester

: 79759-78-7
6-Chloro-1-(2,6-dimethyl-phenyl)-1,3-dihydro-benzoimidazol-2-one

Guidance literature:: With sodium ethanolate; In ethanol; for 3h; Heating;

Reference yield:

: 610-40-2
3,4-dinitro-chlorobenzene

: 79759-78-7
6-Chloro-1-(2,6-dimethyl-phenyl)-1,3-dihydro-benzoimidazol-2-one

Guidance literature:: Multi-step reaction with 4 steps

1: 50 percent / ethanol / 16 h / Heating

2: 76 percent / 37 percent aq. HCl, zinc powder / ethanol / 1 h

3: 82 percent / CHCl₃ / 6 h / Heating

4: 76 percent / EtONa / ethanol / 3 h / Heating

With hydrogenchloride; sodium ethanolate; zinc; In ethanol; chloroform;

Reference yield:

: 79759-09-4
4-Chloro-N²-(2,6-dimethyl-phenyl)-benzene-1,2-diamine

: 79759-78-7
6-Chloro-1-(2,6-dimethyl-phenyl)-1,3-dihydro-benzoimidazol-2-one

Guidance literature:: Multi-step reaction with 2 steps

1: 82 percent / CHCl₃ / 6 h / Heating

2: 76 percent / EtONa / ethanol / 3 h / Heating

With sodium ethanolate; In ethanol; chloroform;