1,3-Dihydro-5-chloro-3-(2,6-dimethylphenyl)-1-methyl-2H-benzimidazol-2-one

Base Information

Chemical Name:1,3-Dihydro-5-chloro-3-(2,6-dimethylphenyl)-1-methyl-2H-benzimidazol-2-one
CAS No.:79759-79-8
Molecular Formula:C16H15ClN2O
Molecular Weight:286.7561
Hs Code.:
DSSTox Substance ID:DTXSID301000713
Wikidata:Q82994415

Synonyms:BRN 5578199;1,3-Dihydro-5-chloro-3-(2,6-dimethylphenyl)-1-methyl-2H-benzimidazol-2-one;2H-Benzimidazol-2-one, 1,3-dihydro-5-chloro-3-(2,6-dimethylphenyl)-1-methyl-;79759-79-8;DTXSID301000713;LS-33306;5-Chloro-3-(2,6-dimethylphenyl)-1-methyl-1,3-dihydro-2H-benzimidazol-2-one

Suppliers and Price of 1,3-Dihydro-5-chloro-3-(2,6-dimethylphenyl)-1-methyl-2H-benzimidazol-2-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of 1,3-Dihydro-5-chloro-3-(2,6-dimethylphenyl)-1-methyl-2H-benzimidazol-2-one

Chemical Property:

Vapor Pressure:2.13E-07mmHg at 25°C
Boiling Point:424.1°Cat760mmHg
Flash Point:210.3°C
Density:1.269g/cm³
XLogP3:3.8
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:1
Exact Mass:286.0872908
Heavy Atom Count:20
Complexity:379

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=C(C(=CC=C1)C)N2C3=C(C=CC(=C3)Cl)N(C2=O)C

Technology Process of 1,3-Dihydro-5-chloro-3-(2,6-dimethylphenyl)-1-methyl-2H-benzimidazol-2-one

There total 6 articles about 1,3-Dihydro-5-chloro-3-(2,6-dimethylphenyl)-1-methyl-2H-benzimidazol-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 79759-78-7
6-Chloro-1-(2,6-dimethyl-phenyl)-1,3-dihydro-benzoimidazol-2-one

: 74-88-4
methyl iodide

: 79759-79-8
5-Chloro-3-(2,6-dimethyl-phenyl)-1-methyl-1,3-dihydro-benzoimidazol-2-one

Guidance literature:: With sodium hydroxide; In methanol; for 10h; Ambient temperature;

Reference yield:

: 610-40-2
3,4-dinitro-chlorobenzene

: 79759-79-8
5-Chloro-3-(2,6-dimethyl-phenyl)-1-methyl-1,3-dihydro-benzoimidazol-2-one

Guidance literature:: Multi-step reaction with 5 steps

1: 50 percent / ethanol / 16 h / Heating

2: 76 percent / 37 percent aq. HCl, zinc powder / ethanol / 1 h

3: 82 percent / CHCl₃ / 6 h / Heating

4: 76 percent / EtONa / ethanol / 3 h / Heating

5: 72 percent / NaOH / methanol / 10 h / Ambient temperature

With hydrogenchloride; sodium hydroxide; sodium ethanolate; zinc; In methanol; ethanol; chloroform;

Reference yield:

: 79759-09-4
4-Chloro-N²-(2,6-dimethyl-phenyl)-benzene-1,2-diamine

: 79759-79-8
5-Chloro-3-(2,6-dimethyl-phenyl)-1-methyl-1,3-dihydro-benzoimidazol-2-one

Guidance literature:: Multi-step reaction with 3 steps

1: 82 percent / CHCl₃ / 6 h / Heating

2: 76 percent / EtONa / ethanol / 3 h / Heating

3: 72 percent / NaOH / methanol / 10 h / Ambient temperature

With sodium hydroxide; sodium ethanolate; In methanol; ethanol; chloroform;