2-PHENYLSULFONYLPRIDINE

Base Information

• Chemical Name: 2-PHENYLSULFONYLPRIDINE
• CAS No.: 24244-60-8
• Molecular Formula: C11H9NO2S
• Molecular Weight: 219.264
• Mol file: 24244-60-8.mol

Synonyms:2-(Phenylsulfonyl)pyridine;2-Benzenesulfonylpyridine;2-Pyridyl phenyl sulfone;NSC 152132;NSC 633011;

Chemical Property of 2-PHENYLSULFONYLPRIDINE

Chemical Property:

• Vapor Pressure: 1.8E-06mmHg at 25°C
• Melting Point: 93-95 °C
• Refractive Index: 1.594
• Boiling Point: 407.3 °C at 760mmHg
• PKA: -1.84±0.19(Predicted)
• Flash Point: 200.1 °C
• PSA: 55.41000
• Density: 1.282 g/cm³
• LogP: 2.99520
• Storage Temp.: Sealed in dry,Room Temperature

Purity/Quality:

98% ^*data from raw suppliers

2-(Phenylsulfonyl)pyridine ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Uses: 2-(Phenylsulfonyl)pyridine is a useful building block in organic synthesis.

Technology Process of 2-PHENYLSULFONYLPRIDINE

There total 28 articles about 2-PHENYLSULFONYLPRIDINE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

crotonaldehyde (2-butenal) + benzenesulfonyl cyanide (24224-99-5) → 2-(phenylsulfonyl)pyridine (24244-60-8)

Guidance literature:

With lithium perchlorate; In toluene; butan-1-ol;

Reference yield: 99.0%

trans-Crotonaldehyde (123-73-9,4170-30-3) + boric acid tributyl ester (688-74-4) + benzenesulfonyl cyanide (24224-99-5) → 2-(phenylsulfonyl)pyridine (24244-60-8)

Guidance literature:

In di-isopropyl ether; butan-1-ol;

Reference yield: 99.0%

trans-Crotonaldehyde (123-73-9,4170-30-3) + phosphoric acid tributyl ester (126-73-8) + benzenesulfonyl cyanide (24224-99-5) → 2-(phenylsulfonyl)pyridine (24244-60-8)

Guidance literature:

In toluene; butan-1-ol;

upstream raw materials:

benzenesulfonyl cyanide

trans-Crotonaldehyde

phosphoric acid tributyl ester

boric acid tributyl ester

Downstream raw materials:

(2-chlorophenyl)[2-(phenylsulfonyl)pyridin-3-yl]methanol

2-((2R,3R)-3-(tert-butyl)-4-methoxy-2,3-dihydrobenzo[d][1,3]oxaphosphol-2-yl)pyridine

2-((2R,3R)-3-(tert-butyl)-4-(2,6-dimethoxyphenyl)-2,3-dihydrobenzo[d][1,3]oxaphosphol-2-yl)pyridine

2-((2R,3R)-4-(anthracen-9-yl)-3-(tert-butyl)-2,3-dihydrobenzo[d][1,3]oxaphosphol-2-yl)pyridine