Technology Process of 2-Hexenoic acid, 4-hydroxy-6-(2-methyl-1,3-dithian-2-yl)-, phenylmethyl
ester, (2E)-
There total 6 articles about 2-Hexenoic acid, 4-hydroxy-6-(2-methyl-1,3-dithian-2-yl)-, phenylmethyl
ester, (2E)- which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 80 percent / diethyl ether / 0.25 h / -78 °C
2: 98 percent / BF3*Et2O / CH2Cl2 / 3 h / 20 °C
3: 92 percent / SO3*pyridine; Et3N / dimethylsulfoxide; CH2Cl2 / 3 h / 20 °C
4: 3.144 g / piperidine / acetonitrile / 15 h / 20 °C
With
piperidine; pyridine-SO3 complex; boron trifluoride diethyl etherate; triethylamine;
In
diethyl ether; dichloromethane; dimethyl sulfoxide; acetonitrile;
DOI:10.1016/j.tet.2006.09.061
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 98 percent / BF3*Et2O / CH2Cl2 / 3 h / 20 °C
2: 92 percent / SO3*pyridine; Et3N / dimethylsulfoxide; CH2Cl2 / 3 h / 20 °C
3: 3.144 g / piperidine / acetonitrile / 15 h / 20 °C
With
piperidine; pyridine-SO3 complex; boron trifluoride diethyl etherate; triethylamine;
In
dichloromethane; dimethyl sulfoxide; acetonitrile;
DOI:10.1016/j.tet.2006.09.061
