3-(Benzyloxy)-2-methylbenzaldehyde

Base Information

Chemical Name:3-(Benzyloxy)-2-methylbenzaldehyde
CAS No.:918524-14-8
Molecular Formula:C15H14O2
Molecular Weight:226.275
Hs Code.:
DSSTox Substance ID:DTXSID30580249
Nikkaji Number:J1.383.174B
Wikidata:Q82471029

Synonyms:3-(Benzyloxy)-2-methylbenzaldehyde;918524-14-8;3-Benzyloxy-2-methyl-benzaldehyde;2-methyl-3-phenylmethoxybenzaldehyde;SCHEMBL410058;3-Benzyloxy-2-methylbenzaldehyde;DTXSID30580249;CZJBHJJWANLNGM-UHFFFAOYSA-N;CS-0196231;E92118;A1-11216

Suppliers and Price of 3-(Benzyloxy)-2-methylbenzaldehyde

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 4 raw suppliers

Chemical Property of 3-(Benzyloxy)-2-methylbenzaldehyde

Chemical Property:

XLogP3:3.2
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:4
Exact Mass:226.099379685
Heavy Atom Count:17
Complexity:233

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=C(C=CC=C1OCC2=CC=CC=C2)C=O

Technology Process of 3-(Benzyloxy)-2-methylbenzaldehyde

There total 5 articles about 3-(Benzyloxy)-2-methylbenzaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 918524-13-7
(3-(benzyloxy)-2-methylphenyl)methanol

: 918524-14-8
3-(benzyloxy)-2-methylbenzaldehyde

Guidance literature:: With Dess-Martin periodane; In tetrahydrofuran; at 0 ℃; for 0.833333h;

Reference yield:

: 100-39-0
benzyl bromide

: 918524-14-8
3-(benzyloxy)-2-methylbenzaldehyde

Guidance literature:: Multi-step reaction with 4 steps

1.1: potassium carbonate / N,N-dimethyl-formamide / 3 h / 10 - 35 °C

2.1: sodium hydroxide; water / tetrahydrofuran; methanol / 3 h / 10 - 35 °C

3.1: borane tetrahydrofuran / tetrahydrofuran / 2.5 h / 10 - 35 °C

3.2: Cooling with ice

4.1: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / dimethyl sulfoxide / 2 h / 10 - 35 °C

With water; borane tetrahydrofuran; potassium carbonate; sodium hydroxide; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In tetrahydrofuran; methanol; dimethyl sulfoxide; N,N-dimethyl-formamide;

Reference yield:

: 208986-50-9
3-(benzyloxy)-2-methylbenzoic acid

: 918524-14-8
3-(benzyloxy)-2-methylbenzaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1.1: borane tetrahydrofuran / tetrahydrofuran / 2.5 h / 10 - 35 °C

1.2: Cooling with ice

2.1: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / dimethyl sulfoxide / 2 h / 10 - 35 °C

With borane tetrahydrofuran; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In tetrahydrofuran; dimethyl sulfoxide;