2,2-Dichloro-1-(4-ethoxyphenyl)cyclopropane-1-carbonyl chloride

Base Information

Chemical Name:2,2-Dichloro-1-(4-ethoxyphenyl)cyclopropane-1-carbonyl chloride
CAS No.:91852-63-0
Molecular Formula:C12H11Cl3O2
Molecular Weight:293.57400
Hs Code.:
DSSTox Substance ID:DTXSID60516071
Nikkaji Number:J135.063C
Mol file:91852-63-0.mol

Synonyms:91852-63-0;2,2-Dichloro-1-(4-ethoxyphenyl)cyclopropane-1-carbonyl chloride;SCHEMBL10585508;DTXSID60516071;PADSRMKFROZNET-UHFFFAOYSA-N;2,2-dichloro-1-(4-ethoxyphenyl)cyclopropanecarbonyl chloride;1-p-Ethoxyphenyl-2,2-dichlorocyclopropane-1-carbonyl chloride;(+/-)-1-(4-ethoxyphenyl)-2,2-dichlorocyclopropane-1-carboxylic acid chloride

Suppliers and Price of 2,2-Dichloro-1-(4-ethoxyphenyl)cyclopropane-1-carbonyl chloride

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of 2,2-Dichloro-1-(4-ethoxyphenyl)cyclopropane-1-carbonyl chloride

Chemical Property:

PSA：26.30000
LogP:3.66610
XLogP3:3.9
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:4
Exact Mass:291.982463
Heavy Atom Count:17
Complexity:311

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCOC1=CC=C(C=C1)C2(CC2(Cl)Cl)C(=O)Cl

Technology Process of 2,2-Dichloro-1-(4-ethoxyphenyl)cyclopropane-1-carbonyl chloride

There total 6 articles about 2,2-Dichloro-1-(4-ethoxyphenyl)cyclopropane-1-carbonyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 103-73-1
Phenetole

: 91852-63-0
1-(4-ethoxyphenyl)-2,2-dichlorocyclopropane-1-carboxylic acid chloride

Guidance literature:: Multi-step reaction with 5 steps

1: 85 percent / Al₂O₃ / TiCl₄ / CH₂Cl₂ / 8 h / -15 °C

2: 100 percent / p-TsOH; hydroquinone / toluene / 3 h / Heating

3: 4.95 g / KF; Al₂O₃ / acetonitrile; H₂O / 20 °C

4: 95 percent / aq. NaOH / methanol / 3 h / Heating

5: SOCl₂ / 1 h / Heating

With aluminum oxide; potassium fluoride; sodium hydroxide; thionyl chloride; toluene-4-sulfonic acid; hydroquinone; titanium tetrachloride; In methanol; dichloromethane; water; toluene; acetonitrile; 1: Friedel-Crafts reaction;
DOI:10.1002/adsc.200505450