2-Propenoic acid, 3-[2-[2-[[(1,1-dimethylethoxy)carbonyl]amino]ethyl]-5-methoxy-4-(phenyl methoxy)phenyl]-, ethyl ester, (2E)-

Base Information

Chemical Name:2-Propenoic acid, 3-[2-[2-[[(1,1-dimethylethoxy)carbonyl]amino]ethyl]-5-methoxy-4-(phenyl methoxy)phenyl]-, ethyl ester, (2E)-
CAS No.:918896-61-4
Molecular Formula:C₂₆H₃₃NO₆
Molecular Weight:455.551
Hs Code.:

Synonyms:

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Chemical Property of 2-Propenoic acid, 3-[2-[2-[[(1,1-dimethylethoxy)carbonyl]amino]ethyl]-5-methoxy-4-(phenyl methoxy)phenyl]-, ethyl ester, (2E)-

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2-Propenoic acid, 3-[2-[2-[[(1,1-dimethylethoxy)carbonyl]amino]ethyl]-5-methoxy-4-(phenyl methoxy)phenyl]-, ethyl ester, (2E)-

There total 7 articles about 2-Propenoic acid, 3-[2-[2-[[(1,1-dimethylethoxy)carbonyl]amino]ethyl]-5-methoxy-4-(phenyl methoxy)phenyl]-, ethyl ester, (2E)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 918896-59-0
1-benzyloxy-4-bromo-2-methoxy-5-(2-nitro ethyl)benzene

: 918896-61-4
2-[2-(ethylpropionate)-4-methoxy-5-benzyloxy]-1-(tert-butoxycarbonyl-amino)-ethane

Guidance literature:: Multi-step reaction with 3 steps

1: lithium aluminum hydride / tetrahydrofuran / 20 °C

2: 1.90 g / tetrahydrofuran; H₂O / 4 h / 20 °C

3: 89 percent / triethylamine; poly(ethylene glycol) / palladium(II) acetate / 18 h / 80 °C

With lithium aluminium tetrahydride; ethylene glycol; triethylamine; poly(ethylene glycol); palladium diacetate; In tetrahydrofuran; water; 3: Heck reaction;
DOI:10.1016/j.tet.2006.09.056

Reference yield:

: 2973-59-3
2-bromoisovanillin

: 918896-61-4
2-[2-(ethylpropionate)-4-methoxy-5-benzyloxy]-1-(tert-butoxycarbonyl-amino)-ethane

Guidance literature:: Multi-step reaction with 6 steps

1: 90 percent / potassium carbonate / acetone / 4 h / Heating

2: 85 percent / ammonium acetate; acetic acid / 4 h / 100 °C

3: 80 percent / sodium borohydride / ethanol / 2 h / 0 °C

4: lithium aluminum hydride / tetrahydrofuran / 20 °C

5: 1.90 g / tetrahydrofuran; H₂O / 4 h / 20 °C

6: 89 percent / triethylamine; poly(ethylene glycol) / palladium(II) acetate / 18 h / 80 °C

With ammonium acetate; sodium tetrahydroborate; lithium aluminium tetrahydride; potassium carbonate; ethylene glycol; acetic acid; triethylamine; poly(ethylene glycol); palladium diacetate; In tetrahydrofuran; ethanol; water; acetone; 2: aldol condensation / 6: Heck reaction;
DOI:10.1016/j.tet.2006.09.056

Reference yield:

: 5392-10-9
2-bromo-4,5-dimethoxybenzaldehyde

: 918896-61-4
2-[2-(ethylpropionate)-4-methoxy-5-benzyloxy]-1-(tert-butoxycarbonyl-amino)-ethane

Guidance literature:: Multi-step reaction with 7 steps

1: 85 percent / sulfuric acid / 6 h / 90 °C

2: 90 percent / potassium carbonate / acetone / 4 h / Heating

3: 85 percent / ammonium acetate; acetic acid / 4 h / 100 °C

4: 80 percent / sodium borohydride / ethanol / 2 h / 0 °C

5: lithium aluminum hydride / tetrahydrofuran / 20 °C

6: 1.90 g / tetrahydrofuran; H₂O / 4 h / 20 °C

7: 89 percent / triethylamine; poly(ethylene glycol) / palladium(II) acetate / 18 h / 80 °C

With ammonium acetate; sodium tetrahydroborate; lithium aluminium tetrahydride; sulfuric acid; potassium carbonate; ethylene glycol; acetic acid; triethylamine; poly(ethylene glycol); palladium diacetate; In tetrahydrofuran; ethanol; water; acetone; 3: aldol condensation / 7: Heck reaction;
DOI:10.1016/j.tet.2006.09.056